Citation: XU Wen, ZHOU Xun, XU Jin-Ming, XU Han, TAO Fei-Fei. Electrochemical Sensor Based on Ni₁₂P₅ Nanoparticles for Sensitive Determination of Glucose[J]. Chinese Journal of Inorganic Chemistry, ;2019, 35(4): 729-736. doi: 10.11862/CJIC.2019.073 shu

Electrochemical Sensor Based on Ni₁₂P₅ Nanoparticles for Sensitive Determination of Glucose

XU Wen ¹ ,
ZHOU Xun ² ,
XU Jin-Ming ¹ ,
XU Han ¹ ,
TAO Fei-Fei ^3,,

1.
School of Chemistry and Chemical Engineering, Key Laboratory of Inorgnic Functional Material, Huangshan University, Huangshan, Anhui 245041, China
2.
Analysis and Testing Center, Huangshan University, Huangshan, Anhui 245041, China
3.
Department of Chemistry and Chemical Engineering, Shaoxing University, Shaoxing, Zhejiang 312000, China

Corresponding author: TAO Fei-Fei, feifeitao@usx.edu.cn
Received Date: 21 November 2018
Revised Date: 8 January 2019

Figures(6)

A non-enzymatic glucose biosensor was designed for the first time based on the employment of monodisperse Ni₁₂P₅ nanoparticles (NPs), which were fabricated by a modified one-pot hot-solution colloidal preparation method. The crystal structure, chemical composition and morphology of the Ni₁₂P₅ NPs was determined by using power X-ray diffraction, transmission electron microscopy, X-ray photoelectron spectra, X-ray energy dispersive spectrometer. The developed sensor has presented excellent performance which involved a quick response time less than 3 s, a broad detection ranging from 0.002 to 4.2 mmol·L^-1, a high sensitivity up to 1 572 mA·L·mol^-1·cm^-2, and a detection limit as low as 0.8 μmol·L^-1. Additionally, it can be used to detect the glucose in the human blood serum with satisfactory result.
- nanoparticles,
- biosensor,
- glucose,
- electroanalysis
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通讯作者: 陈斌, bchen63@163.com

Electrochemical Sensor Based on Ni₁₂P₅ Nanoparticles for Sensitive Determination of Glucose