Citation: DING Hou-Yuan, SHANG Shao-Ming, QIN Gao-Min, ZHAO Bei-Bei, LIU Hao, GU Dan. Submicron Tetragonal Barium Titanate: Preparation by Solid State Reaction at Low Temperature and Crystal Phase Control[J]. Chinese Journal of Inorganic Chemistry, ;2018, 34(8): 1483-1488. doi: 10.11862/CJIC.2018.171 shu

Submicron Tetragonal Barium Titanate: Preparation by Solid State Reaction at Low Temperature and Crystal Phase Control

School of Chemical and Material Engineering, Jiangnan University, Wuxi, Jiangsu 214122, China

Corresponding author: SHANG Shao-Ming, smshang@jiangnan.edu.cn
Received Date: 28 March 2018
Revised Date: 23 April 2018

Figures(5)

Submicron barium titanate with spherical morphology was synthesized at relatively low temperature by using barium hydroxide octahydrate and α-titanic acid as starting materials. Barium titanate samples were characterized by XRD, SEM, Raman and FTIR, and the results show that the samples have high crystallinity and good uniformity. Tetragonal phase-based barium titanate can be obtained by phase transition from cubic phase-based barium titanate at low temperatue of 400℃. The preliminarily results of phase transition study were indicated.
- tetragonal barium titanate,
- low temperature solid state reaction,
- phase transition,
- submicron,
- controllable crystal phase,
- inorganic functional powder
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沈阳化工大学材料科学与工程学院沈阳 110142