Citation: GUO Shuai-Long, CHAO Yun-Xiu, YANG Hong-Wei, YANG Yu-Wen, LI Yu-Xiu, FANG Wei. Preparation and Catalytic Activity of Three-Dimensional Highly Branched Snowflake-like Silver[J]. Chinese Journal of Inorganic Chemistry, ;2018, 34(3): 421-426. doi: 10.11862/CJIC.2018.040 shu

Preparation and Catalytic Activity of Three-Dimensional Highly Branched Snowflake-like Silver

State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals, Kunming Institute of Precious Metals, Kunming 650106, China

Corresponding author: FANG Wei, yhw@ipm.com.cn
Received Date: 16 August 2017
Revised Date: 25 October 2017

Figures(6)

Three-dimensional highly branched snowflake-like silver powder (3DHBS) has been one-step synthesized by reducing silver nitrate with ascorbic acid under the protection of polyvinyl alcohol in aqueous solution at room temperature. The microstructure of 3DHBS was investigated in details through different characteristic methods including X-ray diffraction (XRD) and scanning electron microscopy (SEM), and the possible formation mechanism was proposed based upon it. Additionally, 3DHBS exhibits superior catalytic activity for the hydrogenation reduction of p-nitrophenol.
- silver powder,
- polyvinyl alcohol,
- ascorbic acid,
- 4-nitrophenol,
- hydrogenation reduction
1. [1]
  Chia M Y, Chiu W S, Daud S N H, et al. Mater. Charact., 2015, 106:185-194 doi: 10.1016/j.matchar.2015.05.031
2. [2]
  Park S K, Choi K, Lee S H, et al. Carbon, 2017, 116:500-509 doi: 10.1016/j.carbon.2017.02.024
3. [3]
  Zhao R, Fu G, Zhou T, et al. Nanoscale, 2014, 6(5):2776-2781 doi: 10.1039/c3nr05718f
4. [4]
  Lu H, Zhang H, Yu X, et al. Plasmonics, 2012, 7(1):167-173 doi: 10.1007/s11468-011-9290-8
5. [5]
  HUANG Fu-Chun, LI Wen-Lin, XIONG Qing-Feng, et al. Precious Met., 2012, 33(2):30-35
6. [6]
  Yang J, Lu L, Wang H, et al. Cryst. Growth Des., 2006, 6(9):2155-2158 doi: 10.1021/cg060143i
7. [7]
  WANG Jing, WANG Hui, JING Xiao-Lian, et al. China Sciencepaper, 2015, 10(6):629-632
8. [8]
  SHI Chang-Kuai, LIANG Shi-Yu, ZHU Xiao-Yun. Rare Met., 2015, 39(6):533-539
9. [9]
  Zhai A X, Cai X H, Bin D U. Trans. Nonferrous Met. Soc. China, 2014, 24(5):1452-1457 doi: 10.1016/S1003-6326(14)63212-X
10. [10]
  SONG Yong-Hui, LIANG Gong-Ying, ZHANG Qiu-Li, et al. Rare Met. Mater. Eng., 2007, 36(4):709-712
11. [11]
  Song Y H, Zhou J T, Lan X Z, et al. Adv. Mater. Res., 2011, 233-235:1911-1915 doi: 10.4028/www.scientific.net/AMR.233-235
12. [12]
  Hild M, Mohammed F A R, Aibibu D, et al. Autex Res. J., 2015, 15(1):54-59
13. [13]
  Bleken F L, Chavan S, Olsbye U, et al. Appl. Catal. A, 2012, 447-448(24):178-185
14. [14]
  Burgin J, Florea I, Majimel J, et al. Nanoscale, 2012, 4(4):1299-1303 doi: 10.1039/c2nr11454b
15. [15]
  He Y, Su S, Xu T, et al. Nano Today, 2011, 6(2):122-130 doi: 10.1016/j.nantod.2011.02.004
16. [16]
  Ma X, Guo Q, Xie Y, et al. Chem. Phys. Lett., 2016, 652:148-151 doi: 10.1016/j.cplett.2016.04.004
17. [17]
  Yang C, Cui X, Zhang Z, et al. Nat. Commun., 2015, 6(8150):10-19
18. [18]
  Saha S, Pal A, Kundu S, et al. Langmuir, 2010, 26(4):2885-2893 doi: 10.1021/la902950x
19. [19]
  Liu W, Sun D, Fu J, et al. RSC Adv., 2014, 4(21):11003-11011 doi: 10.1039/C3RA47829G
20. [20]
  Xiong R, Lu C, Wang Y, et al. J. Mater. Chem. A, 2013, 1(47):14910-14918 doi: 10.1039/c3ta13314a
21. [21]
  MENG Xian-Wei, YANG Hong-Wei, HU Chang-Yi, et al. Chinese J. Inorg. Chem., 2016, 32(11):1981-1986
22. [22]
  Choi I H, Kim Y, Lee D N, et al. Polyhedron, 2016, 105:96-103 doi: 10.1016/j.poly.2015.12.022
23. [23]
  Zhang G, Deng C, Shi H, et al. Appl. Surf. Sci., 2017, 402:154-160 doi: 10.1016/j.apsusc.2017.01.042
24. [24]
  Mao Y, Wei J, Wang C, et al. Mater. Lett., 2015, 154(S01):47-50
25. [25]
  And M H R, Mandal T K. J. Phys. Chem. C, 2007, 111(45):16750-16760 doi: 10.1021/jp074963x
26. [26]
  Chi Y, Tu J, Wang M, et al. J. Colloid Interface Sci., 2014, 423(3):54-59
27. [27]
  Chi Y, Yuan Q, Li Y, et al. J. Colloid Interface Sci., 2012, 383(1):96-102 doi: 10.1016/j.jcis.2012.06.027
28. [28]
  Tang S, Vongehr S, Meng X. J. Phys. Chem. C, 2010, 114(2):977-982 doi: 10.1021/jp9102492
29. [29]
  Shin K S, Cho Y K, Chol J Y, et al. Appl. Catal. A, 2012, 413(1):170-175
30. [30]
  Gu S, Wang W, Tan F, et al. Mater. Res. Bull., 2014, 49(1):138-143
1. [1]
  Guimin ZHANG , Wenjuan MA , Wenqiang DING , Zhengyi FU . Synthesis and catalytic properties of hollow AgPd bimetallic nanospheres. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 963-971. doi: 10.11862/CJIC.20230293
2. [2]
  Jie ZHANG , Xin LIU , Zhixin LI , Yuting PEI , Yuqi YANG , Huimin LI , Zhiqiang LIU . Assembling a luminescence silencing system based on post-synthetic modification strategy: A highly sensitive and selective turn-on metal-organic framework probe for ascorbic acid detection. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 823-833. doi: 10.11862/CJIC.20230310
3. [3]
  Yi YANG , Shuang WANG , Wendan WANG , Limiao CHEN . Photocatalytic CO₂ reduction performance of Z-scheme Ag-Cu₂O/BiVO₄ photocatalyst. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 895-906. doi: 10.11862/CJIC.20230434
4. [4]
  Hailang JIA , Hongcheng LI , Pengcheng JI , Yang TENG , Mingyun GUAN . Preparation and performance of N-doped carbon nanotubes composite Co₃O₄ as oxygen reduction reaction electrocatalysts. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 693-700. doi: 10.11862/CJIC.20230402
5. [5]
  Tong Zhou , Xue Liu , Liang Zhao , Mingtao Qiao , Wanying Lei . Efficient Photocatalytic H₂O₂ Production and Cr(VI) Reduction over a Hierarchical Ti₃C₂/In₄SnS₈ Schottky Junction. Acta Physico-Chimica Sinica, 2024, 40(10): 2309020-. doi: 10.3866/PKU.WHXB202309020
6. [6]
  Wenlong LI , Xinyu JIA , Jie LING , Mengdan MA , Anning ZHOU . Photothermal catalytic CO₂ hydrogenation over a Mg-doped In₂O_3-x catalyst. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 919-929. doi: 10.11862/CJIC.20230421
7. [7]
  Gaofeng WANG , Shuwen SUN , Yanfei ZHAO , Lixin MENG , Bohui WEI . Structural diversity and luminescence properties of three zinc coordination polymers based on bis(4-(1H-imidazol-1-yl)phenyl)methanone. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 849-856. doi: 10.11862/CJIC.20230479
8. [8]
  Kun WANG , Wenrui LIU , Peng JIANG , Yuhang SONG , Lihua CHEN , Zhao DENG . Hierarchical hollow structured BiOBr-Pt catalysts for photocatalytic CO₂ reduction. Chinese Journal of Inorganic Chemistry, 2024, 40(7): 1270-1278. doi: 10.11862/CJIC.20240037
9. [9]
  Zhuo WANG , Junshan ZHANG , Shaoyan YANG , Lingyan ZHOU , Yedi LI , Yuanpei LAN . Preparation and photocatalytic performance of CeO₂-reduced graphene oxide by thermal decomposition. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1708-1718. doi: 10.11862/CJIC.20240067
10. [10]
  Zhihuan XU , Qing KANG , Yuzhen LONG , Qian YUAN , Cidong LIU , Xin LI , Genghuai TANG , Yuqing LIAO . Effect of graphene oxide concentration on the electrochemical properties of reduced graphene oxide/ZnS. Chinese Journal of Inorganic Chemistry, 2024, 40(7): 1329-1336. doi: 10.11862/CJIC.20230447
11. [11]
  Xiutao Xu , Chunfeng Shao , Jinfeng Zhang , Zhongliao Wang , Kai Dai . Rational Design of S-Scheme CeO₂/Bi₂MoO₆ Microsphere Heterojunction for Efficient Photocatalytic CO₂ Reduction. Acta Physico-Chimica Sinica, 2024, 40(10): 2309031-. doi: 10.3866/PKU.WHXB202309031
12. [12]
  Zhanggui DUAN , Yi PEI , Shanshan ZHENG , Zhaoyang WANG , Yongguang WANG , Junjie WANG , Yang HU , Chunxin LÜ , Wei ZHONG . Preparation of UiO-66-NH₂ supported copper catalyst and its catalytic activity on alcohol oxidation. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 496-506. doi: 10.11862/CJIC.20230317
13. [13]
  Yingxiao Zong , Yangfei Wei , Xiaoqing Liu , Junke Wang , Huanfang Guo , Junli Wang , Zhuangzhi Shi , Tao Tu , Cheng Yang , Chongyang Wang , Leyong Wang . The 4^th CCL Organic Chemistry Forum held in Zhangye. Chinese Chemical Letters, 2024, 35(8): 109743-. doi: 10.1016/j.cclet.2024.109743
14. [14]
  Jiahong ZHENG , Jiajun SHEN , Xin BAI . Preparation and electrochemical properties of nickel foam loaded NiMoO₄/NiMoS₄ composites. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 581-590. doi: 10.11862/CJIC.20230253
15. [15]
  Zhen Shi , Wei Jin , Yuhang Sun , Xu Li , Liang Mao , Xiaoyan Cai , Zaizhu Lou . Interface charge separation in Cu2CoSnS4/ZnIn2S4 heterojunction for boosting photocatalytic hydrogen production. Chinese Journal of Structural Chemistry, 2023, 42(12): 100201-100201. doi: 10.1016/j.cjsc.2023.100201
16. [16]
  Keke Han , Wenjun Rao , Xiuli You , Haina Zhang , Xing Ye , Zhenhong Wei , Hu Cai . Two new high-temperature molecular ferroelectrics [1,5-3.2.2-Hdabcni]X (X = ClO₄⁻, ReO₄⁻). Chinese Chemical Letters, 2024, 35(6): 108809-. doi: 10.1016/j.cclet.2023.108809
17. [17]
  Zizheng LU , Wanyi SU , Qin SHI , Honghui PAN , Chuanqi ZHAO , Chengfeng HUANG , Jinguo PENG . Surface state behavior of W doped BiVO₄ photoanode for ciprofloxacin degradation. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 591-600. doi: 10.11862/CJIC.20230225
18. [18]
  Xinyu Huai , Jingxuan Liu , Xiang Wu . Cobalt-Doped NiMoO4 Nanosheet for High-performance Flexible Supercapacitor. Chinese Journal of Structural Chemistry, 2023, 42(10): 100158-100158. doi: 10.1016/j.cjsc.2023.100158
19. [19]
  Ying Li , Long-Jie Wang , Yong-Kang Zhou , Jun Liang , Bin Xiao , Ji-Shen Zheng . An improved installation of 2-hydroxy-4-methoxybenzyl (iHmb) method for chemical protein synthesis. Chinese Chemical Letters, 2024, 35(5): 109033-. doi: 10.1016/j.cclet.2023.109033
20. [20]
  Kai Han , Guohui Dong , Ishaaq Saeed , Tingting Dong , Chenyang Xiao . Boosting bulk charge transport of CuWO4 photoanodes via Cs doping for solar water oxidation. Chinese Journal of Structural Chemistry, 2024, 43(2): 100207-100207. doi: 10.1016/j.cjsc.2023.100207

Get Citation

PDF

XML

Metrics

PDF Downloads(5)
Abstract views(1422)
HTML views(122)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142