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Citation: PENG Xiang, CHEN Yu-Jie, LIU Jia-Xiang. Solvothermal Synthesis and Electrical Performance of Cubic ITO Powders[J]. Chinese Journal of Inorganic Chemistry, ;2017, 33(10): 1769-1774. doi: 10.11862/CJIC.2017.224 shu

Solvothermal Synthesis and Electrical Performance of Cubic ITO Powders

Beijing Key Laboratory of Electrochemical Process and Technology for Materials, State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029, China

Corresponding author: LIU Jia-Xiang, ljxpost@263.net
Received Date: 19 April 2017
Revised Date: 23 July 2017

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Using ethylene glycol, ethanol as mixed solvents, cubic shape ITO powders were synthesized. The effect of reaction time, the concentration of NaOH on the phase and the morphology of ITO powders was investigated, and their influence on the electric conductivity and the mechanisms of ITO powders were also discussed. The results show that using the ethylene glycol and ethanol as mixed solvents, V_EG:V_EtOH=4:1, the cubic shape ITO powders with good dispersancy are prepared, the average particle size is 10.7 nm, and the XRD diffraction intensity ratio I₄₀₀/I₂₂₂ gets up to 0.380. when the ethylene glycol and ethanol act as mixed solvents, V_EG:V_EtOH=4:1, and the concentration of NaOH is 0.275 mol·L^-1, the electric conductivity of the powder gets up to the maximum 46.75 mS·cm^-1.
- solvothermal method,
- cubic shape,
- ITO powder,
- electric conductivity
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