Citation: YU Yan-Yan, GUAN Yun-Feng, CONG Ye, YUAN Xiu-Lan, LI Xuan-Ke, ZHANG Jiang. Preparation and Supercapacitive Performances of SiC-CDCs[J]. Chinese Journal of Inorganic Chemistry, ;2017, 33(5): 853-859. doi: 10.11862/CJIC.2017.085 shu

Preparation and Supercapacitive Performances of SiC-CDCs

YU Yan-Yan ¹ ,
GUAN Yun-Feng ¹ ,
CONG Ye ^1,*,, ,
YUAN Xiu-Lan ¹ ,
LI Xuan-Ke ^1,2,*,, ,
ZHANG Jiang ¹

1.
Wuhan University of Science and Technology, College of Chemistry and Chemical Engineering, Hubei Province Key Laboratory of Coal Conversion and New Carbon Materials, Wuhan 430081, China
2.
Hunan University, College of Materials Science and Engineering, Changsha 410082, China

Corresponding author: CONG Ye, congye626@126.com LI Xuan-Ke, xkli8524@sina.com
Received Date: 18 December 2016
Revised Date: 13 March 2017

Figures(9)

Silicon carbide precursors were synthesized by pyrolysis of polycarbosilane (PCS) at higher temperature. Subsequently, silicon carbide-derived carbons (SiC-CDCs) were obtained via chlorination of the SiC precursors at 1 000℃. The microstructure and morphology of the SiC-CDCs were characterized by X-ray diffraction pattern (XRD), Raman spectra, Transmission electron microscope (TEM) and N₂ adsorption-desorption method. The effects of pyrolysis temperature on the crystal phase, morphology, pore size and distribution of the SiC-CDCs were investigated and the electrochemical performances as the electrode of supercapacitors were evaluated. The results show that SiC-CDCs with larger specific surface areas and sub-nanometer pores can be successfully prepared by chlorination of SiC precursors. Meanwhile, the SiC-CDCs exhibit better specific capacitances and supercapacitive performances at different current densities.
- polycarbosilane,
- pyrolysis,
- chlorine etching,
- silicon carbide-derived carbons,
- pore structure,
- supercapacitor
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