Citation: NIU Yi-Fan, YANG Ying, YANG Wen-Tao. Hydrothermal Synthesis and Nanomechanical Performance of One-Dimensional Selenium Nanostructures[J]. Chinese Journal of Inorganic Chemistry, ;2016, 32(12): 2129-2135. doi: 10.11862/CJIC.2016.270 shu

Hydrothermal Synthesis and Nanomechanical Performance of One-Dimensional Selenium Nanostructures

1.
Sino-European Institute of Aviation Engineering, Civil Aviation University of China, Tianjin 300300, China

Corresponding author: NIU Yi-Fan,
Received Date: 25 May 2016
Available Online: 27 September 2016
Fund Project:

One-dimensional trigonal-selenium (t-Se) nanostructures were synthesized using environment-friendly and one-step hydrothermal process, using GeSe₄ glass as raw material in aqueous solution at 80℃. The morphologies and structures of these one-dimensional selenium products were characterized by transmission electron microscope (TEM), Raman spectrometry, scanning electron microscope (SEM) and atomic force microscope (AFM). The experimental results show that the Se nanofibers were grown along[001] direction with a hexagonal cross section. After 144 h of reaction, the length and diameter of Se nanofibers reached millimeter scale and 1~5 μm respectively. AFM based nanoindentation test reported that the hardness and elastic modulus of Se nanofibers were (399.5±20.4) MPa and (1.13±0.05) GPa respectively. The growth speed of Se nanofibers at pH=12.0 (80℃) was faster than that at pH=3.3 and pH=6.3. Se nanofibers were typically 344 μm long and 1.12 μm in diameter after 24 h of reaction in alkaline medium.
- trigonal-selenium;nanofiber;hydrothermal method;nanomechanical properties
1. [1]
  [1] ZHAO Miao(赵渺), YI Shuang-Pin(易双萍), WANG Zhen-Hu(王震虎). J. Funct. Mater. (功能材料), 2011,42(B02):54-57
2. [2]
  [2] GUO Jing(郭静), JIN Jun(靳俊), WEN Zhao-Yin(温兆银), et al. J. Inorg. Mater. (无机材料学报), 2015,30(8):867-871
3. [3]
  [3] Sargent E H. Nat. Photonics., 2012,6(3):133-135
4. [4]
  [4] Kumar S, Scholes G D. Microchim. Acta, 2008,160(3):315-325
5. [5]
  [5] DING Fei(丁菲), YU Jun-Sheng(于俊生). Chinese J. Inorg. Chem. (无机化学学报), 2009,25(4):708-712
6. [6]
  [6] Kundu D, Krumeich F, Nesper R. J. Power Sources, 2013, 15:112-117
7. [7]
  [7] Zhou X M, Gao P, Sun S C, et al. Chem. Mater., 2015,27(19):6730-6736
8. [8]
  [8] Ray C, Dutta S, Sarkar S, et al. RSC Adv., 2013,3(46):24313-24320
9. [9]
  [9] Tian N, Zhou Z Y, Sun S G, et al. Science, 2007,316(5825):732-735
10. [10]
  [10] Pinna N, Garnweitner G, Beato P, et al. Small, 2005,1:112-121
11. [11]
  [11] Chen H, Yoo J B, Liu Y, et al. Electron. Mater. Lett., 2011,7(4):333-336
12. [12]
  [12] LI Zhi-Lin(李志林), HUA Peng-Min(滑鹏敏). Inorg. Chem. Ind. (无机盐工业), 2009,7:32-34
13. [13]
  [13] Liu M H, Chen Y W, Kuo J L, et al. Chem. Commun., 2015, 51(72):13783-13786
14. [14]
  [14] Panahi-Kalamuei M, Panahi-Kalamuei M, Salavati-Niasari M, et al. Ultrason. Sonochem., 2015,23:246-256
15. [15]
  [15] Panahi-Kalamuei M, Salavati-Niasari M, Hosseinpour-Mashkani S M. J. Alloy. Compd., 2014,617:627-632
16. [16]
  [16] Zhu W, Xu H, Wang W, et al. Appl. Phys. A:Mater., 2006, 83(2):281-284
17. [17]
  [17] Oliver W C, Pharr G M. J. Mater. Res., 1992,7(6):1564-1580
18. [18]
  [18] Pokrovski G S, Schott J. Geochim. Cosmochim. Acta, 1998, 62:1631-1642
19. [19]
  [19] Pokrovski G S, Schott J. Geochim. Cosmochim. Acta, 1998, 62:3413-3428
20. [20]
  [20] ZHANG Xu(张旭), XIE Yi(谢毅), XU Fen(徐芬), et al. Chinese J. Inorg. Chem.(无机化学学报), 2003,19(1):77-80
21. [21]
  [21] Mooradian A, Wright G B. The Physics of Selenium & Tellurium, New York:Pergamon, 1967.
22. [22]
  [22] GAO Xue-Yu(高雪玉), YANG Qing-Sheng(杨庆生), LIU Zhi-Yuan(刘志远), et al. Acta Mater. Compos. Sin. (复合材料学报), 2012,29(5):209-214
23. [23]
  [23] Perera G, Doremus R H, Lanford W. J. Am. Ceram. Soc., 1991,74(7):1554-1558
24. [24]
  [24] Bureau B, Troles J, Le Floch M, et al. J. Non-Cryst. Solids, 2003,319(1):145-153
25. [25]
  [25] Boolchand P, Feng X, Bresser W J. J. Non-Cryst. Solids, 2001,293:348-356
26. [26]
  [26] Lucovsky G, Galeener F L, Keezer R C, et al. Phys. Rev. B, 1974,10(12):5134
27. [27]
  [27] Zhu W, Xu H, Wang W, et al. Appl. Phys. A:Mater., 2006, 83:281-284
28. [28]
  [28] Studart A R, Amstad E, Gauckler L J. Langmuir, 2007,23(3):1081-1090
29. [29]
  [29] Song J M, Zhu J H, Yu S H. J. Phys. Chem. B, 2006,110:23790-23795
30. [30]
  [30] Ogorelec Z, Tonejc A. Mater. Lett., 2000,42:81-85
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沈阳化工大学材料科学与工程学院沈阳 110142