Citation: MENG Xian-Wei, YANG Hong-Wei, HU Chang-Yi, MAO Yong-Yun, YANG Yu-Wen, CHEN Jia-Lin, . Flower-like Silver Sphere Catalytic Material:Preparation and Catalytic Activity for the Hydrogenation Reduction of p-Nitrophenol[J]. Chinese Journal of Inorganic Chemistry, ;2016, 32(11): 1981-1986. doi: 10.11862/CJIC.2016.249
-
The flower-like silver sphere structure has been rapidly synthesized by self-assembly of silver nanoflakes through one-step direct mixing of silver nitrate aqueous solution and an aqueous solution containing ferrous sulfate and citric acid. The influence of dropping speed of silver nitrate aqueous solution and the dosage of citric acid on the morphology and size of product were investigated in details through different characteristic methods including X-ray diffraction (XRD) and scanning electron microscopy (SEM). Furthermore, the possible formation mechanism of flower-like silver sphere was explored. The obtained experimental results indicated that the morphology of silver particles could transform from thin flake into flower-like sphere by simply adjusting the dropping speed of silver nitrate aqueous solution. Additionally, this type of nanomaterial exhibited superior catalytic activity for the hydrogenation reduction of p-nitrophenol.
-
-
[1]
[1] Xia Y, Yang P, Sun Y, et al. Adv. Mater., 2003,34(22):353-389
-
[2]
[2] Hu L, Kim H S, Lee J Y, et al. ACS Nano, 2010,4(5):2955-2963
-
[3]
[3] Peng P, Huang H, Hu A, et al. J. Mater. Chem., 2012,22(26):12997-13001
-
[4]
[4] WEI Zhi-Qiang(魏志强), WEN Xian-Lun(温贤伦), WU Xian-Cheng(吴现成), et al. J. Lanzhou Univ.(兰州大学学报), 2003,39(5):38-40
-
[5]
[5] ZHANG Zhi-Kun(张志琨), CUI Zuo-Lin(崔作林). Nano Technology and Nano Materials(纳米技术与纳米材料). Beijing:National Defence Industry Press, 2000.
-
[6]
[6] PENG Zi-Fei(彭子飞), WANG Guo-Zhong(汪国忠), ZHANG Li-De(张立德), et al. J. Mater. Res.(材料研究学报), 1997,1(1):104-106
-
[7]
[7] SONG Yong-Hui(宋永辉), LIANG Gong-Ying(梁工英), ZHANG Qiu-Li(张秋利), et al. Rare Metal Mater. Eng.(稀有金属材料与工程), 2007,36(4):709-712
-
[8]
[8] Song Y H, Zhou J T, Lan X Z, et al. Adv. Mater. Res., 2011, 233-235:1911-1915
-
[9]
[9] Yun T L, Sang H I, Xia Y N, et al. Chem. Phys. Lett., 2005, 411(4/5/6):479-483
-
[10]
[11] Sun Y G, Xia Y N. Adv. Mater., 2002,14:833-837
-
[11]
[11] HE Hui(何辉), ZHOU Jia-Ting(周家霆), DONG Hong-Jian (董红建), et al. Gold(黄金), 2013,34(1):5-9
-
[12]
[12] ZHANG Bo(张波), ZHAO Ai-Wu(赵爱武), WANG Da-Peng (王大朋), et al. Chem. J. Chinese Universities(高等学校化学学报), 2010,31(8):1491-1495
-
[13]
[13] WU Hui-Jie(吴会杰), ZHANG Jin(张进), WANG Ming-Guang(王明光), et al. J. Chongqing Univ. Arts Sci.(重庆文理学院学报), 2015(2):14-17
-
[14]
[14] Saha S, Pal A, Kundu S, et al. Langmuir, 2010,26:2885-2893
-
[15]
[15] Liu W J, Sun D R, Fu J L, et al. RSC Adv., 2014,4:11003-11011
-
[16]
[16] Xiong R, Lu C H, Wang Y R, et al. J. Mater. Chem. A, 2013, 1:14910-14918
-
[17]
[17] Tang S, Vongehr S, Meng X. J. Phys. Chem. C, 2010,114: 977-982
-
[18]
[18] Mao Y Y, Wei J W, Wang C, et al. Mater. Lett., 2015,154(S01):47-50
-
[19]
[19] Rashid M H, Mandal T K. J. Phys. Chem. C, 2007,111(45): 16750-16760
-
[20]
[20] Chi Y, Yuan Q, Li Y, et al. J. Colloid Interface Sci., 2012, 383(1):96-102
-
[21]
[21] Chi Y, Tu J, Wang M, et al. J. Colloid Interface Sci., 2014, 423(3):54-59
-
[22]
[22] Shin K S, Cho Y K, Choi J Y, et al. Appl. Catal. A:Gen., 2012,413:170-175
-
[23]
[23] Baruah B, Gabriel G J, Akbashev M J, et al. Langmuir, 2013,29(13):4225-4234
-
[24]
[24] Gu S, Wang W, Tan F T, et al. Mater. Res. Bull., 2014,49(1):138-143
-
[25]
[25] Sun Y, Mayers A B, Xia Y. Nano Lett., 2003,3(5):675-679
-
[26]
[26] Qiao Z, Na L, James G, et al. J. Am. Chem. Soc., 2011,133(46):18931-18939
-
[27]
[27] TANG Hui(唐辉). Science & Technology Information(科技信息:学术版), 2006(10):35-36
-
[28]
[28] Yang Y W, Mao Y Y, Wang B, et al. RSC Adv., 2016,6(39): 32430-32433
-
[1]
-
-
[1]
Guimin ZHANG , Wenjuan MA , Wenqiang DING , Zhengyi FU . Synthesis and catalytic properties of hollow AgPd bimetallic nanospheres. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 963-971. doi: 10.11862/CJIC.20230293
-
[2]
Yuhao SUN , Qingzhe DONG , Lei ZHAO , Xiaodan JIANG , Hailing GUO , Xianglong MENG , Yongmei GUO . Synthesis and antibacterial properties of silver-loaded sod-based zeolite. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 761-770. doi: 10.11862/CJIC.20230169
-
[3]
Xiutao Xu , Chunfeng Shao , Jinfeng Zhang , Zhongliao Wang , Kai Dai . Rational Design of S-Scheme CeO2/Bi2MoO6 Microsphere Heterojunction for Efficient Photocatalytic CO2 Reduction. Acta Physico-Chimica Sinica, 2024, 40(10): 2309031-. doi: 10.3866/PKU.WHXB202309031
-
[4]
Yi YANG , Shuang WANG , Wendan WANG , Limiao CHEN . Photocatalytic CO2 reduction performance of Z-scheme Ag-Cu2O/BiVO4 photocatalyst. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 895-906. doi: 10.11862/CJIC.20230434
-
[5]
Hailang JIA , Hongcheng LI , Pengcheng JI , Yang TENG , Mingyun GUAN . Preparation and performance of N-doped carbon nanotubes composite Co3O4 as oxygen reduction reaction electrocatalysts. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 693-700. doi: 10.11862/CJIC.20230402
-
[6]
Tong Zhou , Xue Liu , Liang Zhao , Mingtao Qiao , Wanying Lei . Efficient Photocatalytic H2O2 Production and Cr(VI) Reduction over a Hierarchical Ti3C2/In4SnS8 Schottky Junction. Acta Physico-Chimica Sinica, 2024, 40(10): 2309020-. doi: 10.3866/PKU.WHXB202309020
-
[7]
Wenlong LI , Xinyu JIA , Jie LING , Mengdan MA , Anning ZHOU . Photothermal catalytic CO2 hydrogenation over a Mg-doped In2O3-x catalyst. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 919-929. doi: 10.11862/CJIC.20230421
-
[8]
Gaofeng WANG , Shuwen SUN , Yanfei ZHAO , Lixin MENG , Bohui WEI . Structural diversity and luminescence properties of three zinc coordination polymers based on bis(4-(1H-imidazol-1-yl)phenyl)methanone. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 849-856. doi: 10.11862/CJIC.20230479
-
[9]
Kun WANG , Wenrui LIU , Peng JIANG , Yuhang SONG , Lihua CHEN , Zhao DENG . Hierarchical hollow structured BiOBr-Pt catalysts for photocatalytic CO2 reduction. Chinese Journal of Inorganic Chemistry, 2024, 40(7): 1270-1278. doi: 10.11862/CJIC.20240037
-
[10]
Zhuo WANG , Junshan ZHANG , Shaoyan YANG , Lingyan ZHOU , Yedi LI , Yuanpei LAN . Preparation and photocatalytic performance of CeO2-reduced graphene oxide by thermal decomposition. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1708-1718. doi: 10.11862/CJIC.20240067
-
[11]
Wenjiang LI , Pingli GUAN , Rui YU , Yuansheng CHENG , Xianwen WEI . C60-MoP-C nanoflowers van der Waals heterojunctions and its electrocatalytic hydrogen evolution performance. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 771-781. doi: 10.11862/CJIC.20230289
-
[12]
Zhihuan XU , Qing KANG , Yuzhen LONG , Qian YUAN , Cidong LIU , Xin LI , Genghuai TANG , Yuqing LIAO . Effect of graphene oxide concentration on the electrochemical properties of reduced graphene oxide/ZnS. Chinese Journal of Inorganic Chemistry, 2024, 40(7): 1329-1336. doi: 10.11862/CJIC.20230447
-
[13]
Yingxiao Zong , Yangfei Wei , Xiaoqing Liu , Junke Wang , Huanfang Guo , Junli Wang , Zhuangzhi Shi , Tao Tu , Cheng Yang , Chongyang Wang , Leyong Wang . The 4th CCL Organic Chemistry Forum held in Zhangye. Chinese Chemical Letters, 2024, 35(8): 109743-. doi: 10.1016/j.cclet.2024.109743
-
[14]
Jiahong ZHENG , Jiajun SHEN , Xin BAI . Preparation and electrochemical properties of nickel foam loaded NiMoO4/NiMoS4 composites. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 581-590. doi: 10.11862/CJIC.20230253
-
[15]
Zhen Shi , Wei Jin , Yuhang Sun , Xu Li , Liang Mao , Xiaoyan Cai , Zaizhu Lou . Interface charge separation in Cu2CoSnS4/ZnIn2S4 heterojunction for boosting photocatalytic hydrogen production. Chinese Journal of Structural Chemistry, 2023, 42(12): 100201-100201. doi: 10.1016/j.cjsc.2023.100201
-
[16]
Keke Han , Wenjun Rao , Xiuli You , Haina Zhang , Xing Ye , Zhenhong Wei , Hu Cai . Two new high-temperature molecular ferroelectrics [1,5-3.2.2-Hdabcni]X (X = ClO4−, ReO4−). Chinese Chemical Letters, 2024, 35(6): 108809-. doi: 10.1016/j.cclet.2023.108809
-
[17]
Zizheng LU , Wanyi SU , Qin SHI , Honghui PAN , Chuanqi ZHAO , Chengfeng HUANG , Jinguo PENG . Surface state behavior of W doped BiVO4 photoanode for ciprofloxacin degradation. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 591-600. doi: 10.11862/CJIC.20230225
-
[18]
Xinyu Huai , Jingxuan Liu , Xiang Wu . Cobalt-Doped NiMoO4 Nanosheet for High-performance Flexible Supercapacitor. Chinese Journal of Structural Chemistry, 2023, 42(10): 100158-100158. doi: 10.1016/j.cjsc.2023.100158
-
[19]
Ying Li , Long-Jie Wang , Yong-Kang Zhou , Jun Liang , Bin Xiao , Ji-Shen Zheng . An improved installation of 2-hydroxy-4-methoxybenzyl (iHmb) method for chemical protein synthesis. Chinese Chemical Letters, 2024, 35(5): 109033-. doi: 10.1016/j.cclet.2023.109033
-
[20]
Kai Han , Guohui Dong , Ishaaq Saeed , Tingting Dong , Chenyang Xiao . Boosting bulk charge transport of CuWO4 photoanodes via Cs doping for solar water oxidation. Chinese Journal of Structural Chemistry, 2024, 43(2): 100207-100207. doi: 10.1016/j.cjsc.2023.100207
-
[1]
Metrics
- PDF Downloads(0)
- Abstract views(373)
- HTML views(47)