Citation: LIU Zhen-Xiang, CHEN Yun, LUO Xiao-Hui, DIAO Yin-Jun, WU Chang-Sheng. Syntheses, Crystals and Luminescence of Silver(Ⅰ) Complexes with Metal-Olefin Binding Interactions[J]. Chinese Journal of Inorganic Chemistry, ;2015, (12): 2291-2297. doi: 10.11862/CJIC.2015.304
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One new alkene complexe of silver(Ⅰ), [AgL(NO3)]n (1), (L=4-allyl-2-methoxyphenyl nicotinate) has been prepared by self-assembly of AgNO3 with 4-allyl-2-methoxyphenyl nicotinate (L) in THF/H2O system. The structures of compounds L and 1 are determined by X-ray diffraction analysis. The crystals of the two compounds belong to the monoclinic space group. Compound L is connected to form a dimer, 2D layer sequentially by the weak C-H…O hydrogen bonds. The structure of 1 consists of 1D left-handed helical chains of [AgL]∞ in which the allyl arms and N atoms are coordinated to silver atoms, and right-handed helical chains of [AgNO3]∞ connecting through the Ag-O weak interactions. Two kinds of helices are connected in …ABAB… fashion to form a 2D achiral layer. Finally, the resulted 2D net extents to the 3D supramolecular architecture by the weak C-H…O interactions. In addition, the photoluminescence of L and 1 has been investigated in detail.
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