Citation: BAI Ya-Dong, ZHENG Jia-Jun, FAN Bin-Bin. One Step Synthesis of SAPO-34 Molecular with Hierarchical Porosity[J]. Chinese Journal of Inorganic Chemistry, ;2015, 31(8): 1505-1510. doi: 10.11862/CJIC.2015.225
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Meso-SAPO-34 molecular sieve was synthesized with TPOAC and colloidal silica as the silica source, the total surface area is up to 649 m2·g-1. The ratio of TPOAC and silica sol was investigated, which affects external surface area of SAPO-34. The structure was determined by XRD, BET, SEM, NH3-TPD, results show that mesoporous SAPO-34 external surface area can be adjusted, more the defect position crystal appearance, reduce the amount of strong acid weak acid, a weak trend.Under the condition of the ration of TPOAC and silica sol was 3:2, reaction time was 10 days and the ratio of nAl2O3:nP2O5:nSi:nTEAOH:nH2O=1:0.9:0.5:2:60, the external surface area of synthetic mesoporous SAPO-34 reaches the maximum, the value is 100 m2·g-1.
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