Citation: DENG Sheng-Jun, ZHENG Qiang, RAO Fu-Yuan, LIN Ling-Zhi, ZHANG Ning. Diphenylphosphine Functionalized Graphite Oxide Loaded with Platinum Complex: Preparation and Catalytic Performance for the Hydrosilylation of Olefins[J]. Chinese Journal of Inorganic Chemistry, ;2015, (6): 1085-1090. doi: 10.11862/CJIC.2015.178
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By supported platinum complex to the graphite oxide carrier modified by diphenylphosphine ligands, a GO-P-Pt catalyst was synthesized. The GO-P-Pt catalyst was characterized by means of elemental analysis, FT-IRand XRD, and tested for the hydrosilylation of olefin with triethoxysilane. The catalytic results shows that GO-P-Pt catalyst possessed a high catalytic activity, and 94.6% conversion of 1-octene and 99.4% selectivity of β-adduct in yield were obtained at 100 ℃ after 180 min. And the selectivity of β-adduct was lower when the aromatic olefins were used as reaction substrates. Additionally, GO-P-Pt catalyst can be recycled four times without significant loss of catalytic activity and selectivity.
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