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Citation: YU Wan-Xue, ZHANG Li, XU Guan-Cheng, ZHANG Yan-Hui, JIA Dian-Zen. Synthesis, Crystal Structure and Properties of Two Mn(Ⅱ) Complexes with4-Acyl-pyrazolone Derivative[J]. Chinese Journal of Inorganic Chemistry, ;2015, (1): 205-212. doi: 10.11862/CJIC.2015.007 shu

Synthesis, Crystal Structure and Properties of Two Mn(Ⅱ) Complexes with4-Acyl-pyrazolone Derivative

  • 1.

    Key Laboratory of Material and Technology for Clean Energy, Ministry of Education, Key Laboratory of Advanced Functional Materials, Autonomous Region, Institute of Applied Chemistry, Xinjiang University, Urumqi 830046, China

  • Corresponding author: ZHANG Li,  JIA Dian-Zen, 
  • Received Date: 8 July 2014
    Available Online: 16 September 2014

    Fund Project: 新疆自治区自然科学基金面上项目(No.2012211A009)资助项目. (No.2012211A009)

  • Two manganese complexes, [Mn2L2(μ-CH3OH)2(CH3OH)2] (1) and {[MnL(μ-CH3OH)]·CH3OH·CHCl3}n (2) (H2L=N-(1-phenyl-3-benzyl-4-propylene-5-pyrazolone)-isonicotinic hydrazide) were synthesized and structurally characterized by elemental analyses, IR spectra, UV-Vis spectra, thermogravimetric analyses and single crystal X-ray diffraction. The results show that the pHvalue of the reaction system has significant effect on the coordination mode of the ligand, which results in a dinuclear structure of 1 and a 2D network of 2. The thermal gravimetric analyses show that 1 is more stable than 2. CCDC: 997907, 1; 997908, 2.
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