Citation: YANG Rui-Huan, ZHANG Chi, HUO Ji-Chuan, QU Peng. Preparation and Study of a Novel Glucoside Aromatic Ester Based Metal Organic Material[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(5): 1073-1078. doi: 10.11862/CJIC.2014.180 shu

Preparation and Study of a Novel Glucoside Aromatic Ester Based Metal Organic Material

1.
1 School of Material Science and Engineering, Southwest University of Science and Technology, Mianyang, Sichuan 621010, China;

Received Date: 8 October 2013
Available Online: 26 December 2013
Fund Project: 四川省科技厅国际合作项目(No.2011HH0020)；西南科技大学博士基金(No.10zx7104)；西南科技大学平台科研基金(No.13zxpt08)。 (No.2011HH0020)；西南科技大学博士基金(No.10zx7104)；西南科技大学平台科研基金(No.13zxpt08)

Dentate organic ester ligandsmethyl glucoside aromatic ester based ligands (MGAE ligand) (C₁₅H₁₈O₉, C₁₅H₁₆O₈, C₂₂H₃₀O₁₄, C₂₃H₂₂O₁₂, C₃₁H₂₆O₁₅ or C₃₉H₃₀O₁₈) with complexation ability were, through the catalysis of triethylamine, synthesized using methyl glucoside and phthalic anhydride as selected raw materials. Then, a series of MGAE ligand based metal-organic coordination compounds were prepared in the involvement of triethylamine as a template agent through complexing the new type of organic ligands with metal salt solution,Then the MGAE ligand based complexes were characterized using FT-IR, XRD, TGA, FSEM, EDS and BET. The results showed that the complexation is chiefly due to the involvement of carbonyl in the MGAE ligand and the performance of complexes is mainly influenced by the MGAE ligands and metal cations.
- methy glucoside;MGAE;MGAE-metal complex;metal organic material
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沈阳化工大学材料科学与工程学院沈阳 110142