Citation: LIU Jie-Xiang, ZHANG Yong-Qing, ZHANG Xiao-Guang, WANG Jian-Long, ZHAO Ling-Feng, YANG Jin, WANG Rui. Preparation and Characterization of Intercalation Materials with Layered Hydroxide Salts (LHS)[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(4): 837-844. doi: 10.11862/CJIC.2014.129 shu

Preparation and Characterization of Intercalation Materials with Layered Hydroxide Salts (LHS)

1.
1 School of Chemical Engineering, Hebei University of Technology, Tianjin 300130, China;

Corresponding author: LIU Jie-Xiang, ZHANG Xiao-Guang,
Received Date: 15 September 2013
Available Online: 18 November 2013
Fund Project: 河北省自然科学基金(No.B2011202118)；山东大学胶体与界面化学教育部重点实验室开放课题(No.201202)；河北省高等学校科学技术研究项目(No.QN20131050) (No.B2011202118)；山东大学胶体与界面化学教育部重点实验室开放课题(No.201202)；河北省高等学校科学技术研究项目(No.QN20131050)“大学生创新创业训练计划”国家级项目(No.201310080018)资助项目。 (No.201310080018)

Intercalation of dodecyl benzene sulphonate (DBS) and sulfobutyl ether β-cyclodextrin (SBE-β-CD) into layered zinc hydroxide nitrate (Zn-LHS) and nickel/zinc hydroxide nitrate (NiZn-LHS) was synthesized by coprecipitation and ion-exchanged methods. The effect of anion concentration and pHvalue on preparation was systematically investigated and compared. The products were characterized by X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and thermogravimetry and differential thermal analysis (TG-DTA), and scanning electron microscope (SEM). The results showed that Zn-LHS-DBS with pure phase and good crystallinity was obtained at DBS concentration of 0.19~0.38 mol·L^-1, pH=6.0~7.0, temperature of hydrothermal treatment of 60~100 ℃ by coprecipitation method. The NiZn-LHS-SBE-β-CD with good structure was prepared by ion-exchanged method. Zn-LHS-SBE-β-CD with pure phase was not successfully prepared by both coprecipitation and ion-exchanged method due to the particular structure of SBE-β-CD and poor hydrothermal stability of Zn-LHS. Furthermore, TG-DTA data indicated that stability of SBE-β-CD and DBSimproved distinctly in the interlayer due to the strong supra-molecular interaction existed between anions and hostlayer of LHS.
- zinc hydroxide nitrate;nickel/zinc hydroxide nitrate;dodecyl benzene sulphonate;sulfobutyl ether β-cyclodextrin;thermostability
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