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Citation: LI Xiao-Long, MA Wei-Min, SUN Yang, SHI Shu-Jun, HAN Feng. Preparation of SrHfO3:Ce Ultramicroballoon Luminous Particles by Unitary Alcohol-Thermal Method[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(3): 536-542. doi: 10.11862/CJIC.2014.066 shu

Preparation of SrHfO3:Ce Ultramicroballoon Luminous Particles by Unitary Alcohol-Thermal Method

  • 1.

    Key Laboratory for Advanced Ceramics and Application of Shenyang, School of Materials Science and Engineering, Shenyang University of Chemical Technology, Shenyang 110142, China

  • Received Date: 3 July 2013
    Available Online: 24 September 2013

    Fund Project: 沈阳市先进陶瓷制备技术及应用重点实验室建设项目(No.F12-259-1-00)资助。 (No.F12-259-1-00)

  • The SrHfO3:Ce ultramicroballoon particles were prepared by unitary alcohol-thermal method, by using Sr(NO3)2 and HfOCl2·8H2O as raw materials, using C2H5OH/H2O as solvent, adding KOH aqueous solution as mineralier and Ce(NO3)3·6H2O as activator. The phase transformation and the morphology of powders were studied by XRD and SEM. The excitation and emission spectra of samples were analyzed by the fluorophotometer. The results show that the powders of SrHfO3:Ce are spherical particles with the size of about 900 nm and good dispersibility under the condition of nSr:nHf=1:1, VC2H5OH:VH2O=4:1, pH=13.5, reacted at 140 ℃ for 4 h. The maximum luminous was obtained at doping of 0.7mol% Ce.
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