Citation: HUANG Qing-Li, ZHU Xia-Shi. Synthesis and Characterization of SERS-Active Silver Nanomaterial[J]. Chinese Journal of Inorganic Chemistry, ;2014, (2): 442-450. doi: 10.11862/CJIC.2014.019
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Three-dimensional (3D) hierarchical silver nanomaterials (HSNs) were prepared by a simple surfactant-free wet-chemical method at room temperature. The as-prepared HSNs exhibit spherical morphologies and are constructed with many 2Dnanoflakes as building blocks. Field emission scanning electron microscopy (FESEM) studies show that diammonium 2-(carboxymethyl)-2-hydroxysuccinate (diammonium hydrogen citrate) (C6H14N2O7) plays a key role in the formation of such HSNs. X-ray diffraction (XRD) and transmission electron microscopy (TEM) results confirm the formation of HSNs. The optical properties and surface-enhanced Raman scattering (SERS) effect were also investigated by UV-Vis and Raman spectra. The HSNs could be served as highly sensitive surface-enhanced Raman scattering (SERS) substrates for chemical detection.
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