Citation: HU Jin-Song, ZAHNG Xu-Jiao, CAI Xiao-Wei, SUN Lin-Xiao, ZAHNG Wen-Hao, SHI Jian-Jun, ZHANG Xaio-Mei, XING Hong-Long, HE Jie. Structure and Fluorescence Property of 2D Interlocked Zn(Ⅱ) Coordination Polymer Constructed by V-Shaped Imidazolyl Ligand[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(3): 654-658. doi: 10.11862/CJIC.2014.014
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A new interlocked 2Dachiral coordination polymers {[Zn(BIDPE)(pim)]·(H2O)}n (1) was prepared under hydrothermal conditions based on V-shaped ligand 4,4'-bis(imidazol-1-yl)diphenyl ether (BIDPE) with aliphatic pimelic acid (H2pim). The complex was characterized by IR spectroscopy, TGA, X-ray powder and single-crystal diffraction. It crystallizes in the monoclinic system, space group P21/c. The neighboring Zn(Ⅱ) ions are linked by BIDPE and pim2-anions to form infinitely 2Dchiral layer, two identical 2Dchiral layers interlocked each other to give 2Dchiral+2Dchiral→2Dchiral sheet. The helical directions of adjacent interlocked 2Dchiral sheets are reverse, which stacked in ABAB mode to form 2Dachiral network. In addition, the solid-state photoluminescent property of 1 was also studied. CCDC: 933583.
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