Citation: Zhaoyu Jin, Renjun Guan, Xin Li, Dunyi Yuan, Panpan Li. Advanced characterization techniques for understanding electrocatalytic behavior of oxidized nitrogen waste upcycling processes[J]. Chinese Chemical Letters, ;2025, 36(7): 110506. doi: 10.1016/j.cclet.2024.110506 shu

Advanced characterization techniques for understanding electrocatalytic behavior of oxidized nitrogen waste upcycling processes

Zhaoyu Jin ^{a, *,} ,
Renjun Guan ^{b, c} ,
Xin Li ^b ,
Dunyi Yuan ^b ,
Panpan Li ^{b, *,}

a.
Institute of Fundamental and Frontier Sciences, University of Electronic Science and Technology of China, Chengdu 611731, China
b.
College of Materials Science and Engineering, Sichuan University, Chengdu 610065, China
c.
Pittsburgh Institute, Sichuan University, Chengdu 610207, China

zjin@uestc.edu.cn

panpanli@scu.edu.cn

Received Date: 14 May 2024
Revised Date: 30 July 2024
Accepted Date: 24 September 2024
Available Online: 26 September 2024

Figures(10)

The management of nitrogenous waste emissions presents significant environmental and health challenges. Efficient and sustainable upcycling strategies are needed to convert waste nitrogen compounds into valuable resources. Electrocatalysis has emerged as a promising solution for waste management, but several challenges remain, including the identification of suitable electrocatalysts and understanding the complex reaction mechanisms. In this review, we focus on the progress in electrocatalytic oxidized nitrogen waste upgrading and utilization, highlighting the application of advanced in situ/operando characterization techniques, including X-ray spectroscopy, scanning electrochemical microscopy and others. These techniques provide valuable insights into the structural and chemical properties of electrocatalysts as well as intermediates during electrochemical reactions, enabling a better understanding of reaction mechanisms and optimization of reaction conditions. The review explores the mechanisms of electrocatalytic upcycling of nitrogenous waste, including nitrate/nitrite reduction, nitric oxide reduction, and carbon dioxide and nitrate co-reduction reactions. Additionally, future research directions and development trends are discussed, offering a relevant guide for the development of sustainable electrocatalytic technologies for waste management and resource recovery.
- Electrocatalysis,
- In situ characterization,
- Nitrogenous waste,
- Ammonia electrosynthesis,
- C-N coupling
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沈阳化工大学材料科学与工程学院沈阳 110142