Citation: Yanxin Jiang, Kwai Wun Cheng, Zhiping Yang, Jun (Joelle) Wang. Pd-catalyzed enantioselective and regioselective asymmetric hydrophosphorylation and hydrophosphinylation of enynes[J]. Chinese Chemical Letters, ;2025, 36(5): 110231. doi: 10.1016/j.cclet.2024.110231 shu

Pd-catalyzed enantioselective and regioselective asymmetric hydrophosphorylation and hydrophosphinylation of enynes

Yanxin Jiang ^a ,
Kwai Wun Cheng ^{a, b} ,
Zhiping Yang ^{a, *,} ,
Jun (Joelle) Wang ^{a, *,}

a.
Department of Chemistry, Hong Kong Baptist University, Hong Kong, China
b.
Department of Chemistry, Graduate School of Science, Kyoto University, Kyoto 6068501, Japan

yangzp@hkbu.edu.hk

junwang@hkbu.edu.hk

Received Date: 26 March 2024
Revised Date: 28 June 2024
Accepted Date: 8 July 2024
Available Online: 14 July 2024

Figures(6)

The chemo-, regio-, and enantio-controlled synthesis of P-chiral phosphines in a general and efficient manner remains a significant synthetic challenge. In this study, a Pd-catalyzed hydrofunctionalization is developed for the highly selective synthesis of P-stereogenic alkenylphosphinates and alkenylphosphine oxides via conjugate addition of enynes. Notably, this methodology is suitable for both phosphine oxide and phosphinate nucleophiles, providing a versatile approach for the construction of diverse P-chiral organophosphosphorus compound.
- Phosphine,
- Enyne,
- Pd catalyst,
- P-chirality,
- Asymmetric catalysis
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沈阳化工大学材料科学与工程学院沈阳 110142