Citation: Chao Lu, Zhi Yang, Yujie Wang, Yun Zhang, Hao Wu, Yi Guo, Wenlong Cai. Ethylene glycol-regulated ammonium vanadate with stable layered structure and favorable interplanar spacing as high-performance cathode for aqueous zinc ion batteries[J]. Chinese Chemical Letters, ;2023, 34(8): 108572. doi: 10.1016/j.cclet.2023.108572 shu

Ethylene glycol-regulated ammonium vanadate with stable layered structure and favorable interplanar spacing as high-performance cathode for aqueous zinc ion batteries

Chao Lu ^{a, b} ,
Zhi Yang ^a ,
Yujie Wang ^{b, *,} ,
Yun Zhang ^c ,
Hao Wu ^c ,
Yi Guo ^d ,
Wenlong Cai ^{c, *,}

a.
School of Mechanical Engineering, Chengdu University, Chengdu 610106, China
b.
Department of Chemistry, College of Resource and Environment, Baoshan University, Baoshan 678000, China
c.
College of Materials Science and Engineering, Sichuan University, Chengdu 610064, China
d.
College of Optoelectronic Engineering, Chengdu University of Information Technology, Chengdu 610225, China

wangyujieufo@163.com

caiwl@scu.edu.cn

Received Date: 11 April 2023
Revised Date: 5 May 2023
Accepted Date: 11 May 2023
Available Online: 17 May 2023

Figures(4)

Ammonium vanadate compounds featuring large capacity, superior rate capability and light weight are regarded as promising cathode materials for aqueous zinc ion batteries (AZIBs). However, the controllable synthesis of desired ammonium vanadates remains a challenge. Herein, various ammonium vanadate compounds were successfully prepared by taking advantage of ethylene glycol (EG) regulated polyol-reduction strategy and solvent effect via hydrothermal reaction. The morphology and crystalline phase of resultant products show an evolution from dendritic (NH₄)₂V₆O₁₆ to rod-like NH₄V₄O₁₀ and finally to lamellar (NH₄)₂V₄O₉ as increasing the amount of EG. Specifically, the NH₄V₄O₁₀ product exhibits a high initial capacity of 427.5 mAh/g at 0.1 A/g and stable cycling with a capacity retention of 90.4% after 5000 cycles at 10 A/g. The relatively excellent electrochemical performances of NH₄V₄O₁₀ can be ascribed to the stable open-framework layered structure, favorable (001) interplanar spacing, and peculiar rod-like morphology, which are beneficial to the highly reversible Zn²⁺ storage behaviors. This work offers a unique way for the rational design of high-performance cathode materials for AZIBs.
- Ammonium vanadate rods,
- Ethylene glycol reduction,
- Zn²⁺ storage,
- Cathode,
- Aqueous zinc ion battery
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