Citation: Yan Gong, Yu Ding, Qi Tang, Fei Lian, Chun Bai, Ruiyi Xie, Haijiao Xie, Xu Zhao. Plasmonic Ag nanoparticles decorated MIL-101(Fe) for enhanced photocatalytic degradation of bisphenol A with peroxymonosulfate under visible-light irradiation[J]. Chinese Chemical Letters, ;2024, 35(1): 108475. doi: 10.1016/j.cclet.2023.108475 shu

Plasmonic Ag nanoparticles decorated MIL-101(Fe) for enhanced photocatalytic degradation of bisphenol A with peroxymonosulfate under visible-light irradiation

Yan Gong ^a ,
Yu Ding ^a ,
Qi Tang ^a ,
Fei Lian ^{a, *,} ,
Chun Bai ^a ,
Ruiyi Xie ^a ,
Haijiao Xie ^b ,
Xu Zhao ^{c, *,}

a.
School of Energy and Environmental Engineering, Hebei University of Technology, Tianjin 300401, China
b.
Hangzhou Yanqu Information Technology Co., Ltd., Hangzhou 310003, China
c.
Key Laboratory of Drinking Water Science and Technology, Research Center for Eco-Environmental Sciences, Chinese Academy of Sciences, Beijing 100085, China

lianfei2000@126.com

zhaoxu@rcees.ac.cn

Received Date: 23 December 2022
Revised Date: 28 March 2023
Accepted Date: 18 April 2023
Available Online: 18 April 2023

Figures(7)

Photocatalytic activation of peroxymonosulfate (PMS) has garnered a lot of interest in the field of wastewater treatment. Herein, a plasmonic Ag nanoparticles decorated MIL-101(Fe) hybrid was synthesized through a photodeposition process. Upon light irradiation, the Ag/MIL-101(Fe) exhibit reinforced photocatalytic activities for elimination of bisphenol A (BPA) with PMS. The optimized 2.0% Ag/MIL-101(Fe) composite presented the highest photocatalytic activity with kinetic constant k of 0.102 min⁻¹, which was about 10-fold of the pristine MIL-101(Fe). Loading of plasmonic Ag into MIL-101(Fe) boosts photoinduced carrier separation and accelerates PMS activation to generate strong oxidative radicals. Photoelectrochemical tests and multiple spectroscopic studies confirmed the promoted charge carrier separation and transfer capability of Ag/MIL-101(Fe). Combining the results of radical trapping experiments and electron spin resonance (ESR), the formed SO₄^•−, ^•OH, ^•O₂⁻ and ¹O₂ had a significant role in the photocatalytic process. According to intermediate study, the degradation pathway was studied, and the possible mechanism was proposed.
- Photocatalysis,
- MOF,
- Peroxymonosulfate,
- Plasmonic Ag,
- BPA
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