Citation: Yongxing Sun, Kaijun Quan, Jia Chen, Hui Li, Xin Li, Zuguang Li, Hongdeng Qiu. Synthesis and modification of spherical/hollow metal-organic frameworks for efficient extraction of sulfonamides in aqueous environments[J]. Chinese Chemical Letters, ;2023, 34(9): 108166. doi: 10.1016/j.cclet.2023.108166 shu

Synthesis and modification of spherical/hollow metal-organic frameworks for efficient extraction of sulfonamides in aqueous environments

Yongxing Sun ^{a, b, 1} ,
Kaijun Quan ^{b, 1} ,
Jia Chen ^b ,
Hui Li ^b ,
Xin Li ^b ,
Zuguang Li ^{a, *,} ,
Hongdeng Qiu ^{b, *,}

a.
College of Chemical Engineering, Zhejiang University of Technology, Hangzhou 310014, China
b.
CAS Key Laboratory of Chemistry of Northwestern Plant Resources and Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, China

lzg@zjut.edu.cn

hdqiu@licp.cas.cn

Received Date: 12 November 2022
Revised Date: 14 January 2023
Accepted Date: 27 January 2023
Available Online: 2 February 2023

Figures(5)

In this study, two novel spherical/hollow metal-organic frameworks were successfully synthesized, and further modified by a mild non-covalent modification strategy with dopamine and 1, 4-benzenedithiol (BDT) as polymeric monomers to obtain pBDT@PDA-Ni-MOF and pBDT@PDA-Ni/Co-MOF, respectively. The results showed that the above MOFs possessed extremely fast adsorption rates and ideal adsorption capacities for sulfonamides (SAs) and the modified MOFs exhibited enhanced adsorption capacities for SAs owing to a large number of additional functional groups. Then, benefit of their regular morphology and size, a facile syringe-assisted dispersive solid phase extraction (S-DSPE) method was developed for efficient detection of SAs, which will provide a powerful tool for monitoring trace level of SAs in aqueous environment.
- Unique spherical/hollow MOFs,
- Copolymer modification,
- Solid phase adsorbents,
- SAs sorptive extraction
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