Citation: Le Zhang, Li-Ying Sun, Jin-Ping Chang, Hui-Yu Xie, Ya-Wen Zhang, Yi-Fan Zhang, Ying-Feng Han. A trefoil-shaped macrocycle with [12]-imidazolium cations[J]. Chinese Chemical Letters, ;2022, 33(10): 4567-4571. doi: 10.1016/j.cclet.2022.01.064 shu

A trefoil-shaped macrocycle with [12]-imidazolium cations

Key Laboratory of Synthetic and Natural Functional Molecule of the Ministry of Education, College of Chemistry and Materials Science, Northwest University, Xi'an 710127, China

yfhan@nwu.edu.cn

Received Date: 27 November 2021
Revised Date: 19 January 2022
Accepted Date: 23 January 2022
Available Online: 31 January 2022

Figures(5)

A trefoil-like two-dimensional (2D) C_3v symmetric organic [12]-imidazolium cation H₁₂–2(PF₆)₁₂ featuring three [4]-imidazolium macrocycles was synthesized in three steps. The reaction of a dodecakis H₁₂–1(PF₆)₁₂ imidazolium salt with Ag₂O resulted in the formation of a hexanuclear Ag^Ⅰ dodecacarbene assembly [Ag₆(1)](PF₆)₆. Upon UV irradiation, the photodimerization of the cinnamic ester pendants of [Ag₆(1)](PF₆)₆ led to the generation of a trefoil-like complex [Ag₆(2)](PF₆)₆ containing three closed metallacycles. Removal of metal ions allowed for the synthesis of the target molecule. All complexes were fully characterized by NMR spectroscopy (¹H, ¹³C{¹H} and 2D NMR) and high-resolution electrospray ionization mass spectrometry (HR-ESI-MS).
- Trefoil-shaped macrocycle,
- N-Heterocyclic carbenes,
- Photochemical reaction,
- Imidazolium
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