Citation: Jingyang Li, Ying He, Yongcun Zou, Yan Yan, Zhiguang Song, Xiaodong Shi. Achieving a stable COF with the combination of "flat" and "twist" large-size rigid synthons for selective gas adsorption and separation[J]. Chinese Chemical Letters, ;2022, 33(6): 3017-3020. doi: 10.1016/j.cclet.2021.12.011 shu

Achieving a stable COF with the combination of "flat" and "twist" large-size rigid synthons for selective gas adsorption and separation

Jingyang Li ^a ,
Ying He ^b ,
Yongcun Zou ^a ,
Yan Yan ^a ,
Zhiguang Song ^{a, *,} ,
Xiaodong Shi ^{b, *,}

a.
State key Laboratory of Supramolecular Structure and Materials, College of Chemistry, Jilin University, Changchun 130012, China
b.
University of South Florida, Tampa, FL 33620, United States

szg@jlu.edu.cn

xmshi@usf.edu

Received Date: 27 September 2021
Revised Date: 28 November 2021
Accepted Date: 5 December 2021
Available Online: 9 December 2021

Figures(4)

A new type of covalent organic framework (COF) was achieved using combination of structrally rigid and conformationally othorganal building blocks. The N-2-aryl-substituted triazole derivative (NAT-CHO) was prepared with co-planar conformation among the three aromatic rings as the "flat" building block. The 4, 4′, 4′′, 4′′′-(ethene-1, 1, 2, 2-tetrayl)tetraaniline) (ETTA) was applied as the "twist" building block. A 2D sheet of network was obtained through imine formation. The resulting NAT-COF gave excellent thermal and chemical stability, survived aqueous solutions from pH 5 to 13. With large-size building blocks, the porous framework NAT-COF gave efficient gas adsorption with excellent selectivity of C3 propane over C1 me-thane, suggesting its potential application for selective gas capture and separation.
- N-2-Aryl triazole,
- ETTA,
- Covalent organic framework,
- Gas adsorption and separation
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