Citation: Tan Ting, Xu Xiaomei, Wan Yiqun. DES-Fe₃O₄ composite for rapid extraction of residual plant growth regulators in edible vegetable oil[J]. Chinese Chemical Letters, ;2019, 30(6): 1182-1185. doi: 10.1016/j.cclet.2019.03.057 shu

DES-Fe₃O₄ composite for rapid extraction of residual plant growth regulators in edible vegetable oil

Tan Ting ^a,b ,
Xu Xiaomei ^c ,
Wan Yiqun ^a,b,c,*,

a.
State Key Laboratory of Food Science and Technology, Nanchang University, Nanchang 330047, China
b.
Center of Analysis and Testing, Nanchang University, Nanchang 330031, China
c.
School of Chemistry, Nanchang University, Nanchang 330031, China

wanyiqun@ncu.edu.cn

Received Date: 24 December 2018
Revised Date: 24 March 2019
Accepted Date: 25 March 2019
Available Online: 5 June 2019

Figures(3)

A rapid DES-Fe₃O₄ microextraction coupled with liquid chromatography method was ingeniously developed for simultaneous control of five typical plant growth regulators in a planting cycle including indole-3-acetic acid, abscisic acid, thidiazuron, 1-naphthylacetic acid and forchlorfenuron. The experiments were carried out with one type of carboxylic acid-assisted deep eutectic solvent (n_ChCl:n_{acetic acid}=1:3) as extractant, coupled with ultrasonic wave extraction for 30 min at bath temperature at 50 C. Under the optimum conditions, good extraction performances of linearities for five plant growth regulators were achieved separately in the range of 0.10-50 mg/L of indole-3-acetic acid, 0.06-50 mg/L of abscisic acid, 0.20-50 mg/L of thidiazuron, 0.50-50 mg/L of 1-naphthylacetic acid and 0.06-50 mg/L of forchlorfenuron and recoveries were ranged from 70.4% to 102.2%. Meanwhile, Fe₃O₄ was preferentially combined with DES in the oil matrix, the advantage of which was pointed to rapid and efficient separation of targeted plant growth regulators from complicated oil matrix. The proposed approach achieved satisfied results and met the monitoring requirements of plant growth regulators control in edible vegetable oil samples.
- DES-Fe₃O₄ composite,
- Deep eutectic solvent,
- Rapid separation,
- Plant growth regulators,
- Edible vegetable oil
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通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

DES-Fe3O4 composite for rapid extraction of residual plant growth regulators in edible vegetable oil

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通讯作者: 陈斌, bchen63@163.com

DES-Fe₃O₄ composite for rapid extraction of residual plant growth regulators in edible vegetable oil