Citation: Xia Shujun, Dong Jing, Chen Yiying, Wang Yiru, Chen Xi. Three dimensional phytic acid-induced graphene as a solid-phase microextraction fiber coating and its analytical applications for nerolidol in tea[J]. Chinese Chemical Letters, ;2018, 29(1): 107-110. doi: 10.1016/j.cclet.2017.10.008 shu

Three dimensional phytic acid-induced graphene as a solid-phase microextraction fiber coating and its analytical applications for nerolidol in tea

Xia Shujun ^a ,
Dong Jing ^a ,
Chen Yiying ^a ,
Wang Yiru ^a,, ,
Chen Xi ^a,b,,

a.
Department of Chemistry and the MOE Key Laboratory of Spectrochemical Analysis & Instrumentation, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen 361005, China
b.
State Key Laboratory of Marine Environmental Science, Xiamen University, Xiamen 361005, China

Corresponding author: Wang Yiru, yrwang@xmu.edu.cn Chen Xi, xichen@xmu.edu.cn
Received Date: 26 June 2017
Revised Date: 2 October 2017
Accepted Date: 11 October 2017
Available Online: 12 January 2017

Figures(3)

In this work, three dimensional phytic acid-induced graphene coating was prepared by hydrothermal synthesis and fabricated on a stainless-steel wire using physical coating method as a solid phase microextraction (SPME) coating. The graphene coating revealed high specific surface area, extraordinary electrical conductivity and excellent chemical stability. Coupled with gas chromatography-flame ionization detector (GC-FID), the home-made phytic acid-induced graphene SPME fiber exhibited excellent extraction efficiency for the analysis of nerolidol in tea samples. Under the optimized conditions, the linear range of working curve was found to be 1-1000 ng/g, and the limit of detection of nerolidol was 0.18 ng/g. The coefficient variation of repeatability for each single fiber and reproducibility for fiber to fiber was less than 3.9% and 8.3%, respectively.
- Phytic acid-induced graphene,
- Solid phase microextraction,
- Gas chromatography,
- Nerolidol,
- Tea
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