Citation: Abdullah Nurul Hidayah, Shameli Kamyar, Abdullah Ezzat Chan, Abdullah Luqman Chuah. A facile and green synthetic approach toward fabrication of starch-stabilized magnetite nanoparticles[J]. Chinese Chemical Letters, ;2017, 28(7): 1590-1596. doi: 10.1016/j.cclet.2017.02.015 shu

A facile and green synthetic approach toward fabrication of starch-stabilized magnetite nanoparticles

a.
Department of Environmental Engineering and Green Technology (EGT), Malaysia-Japan International Institute of Technology (MJIIT), Universiti Teknologi Malaysia (UTM), Jalan Sultan Yahya Petra, Kuala Lumpur 54100, Malaysia
b.
Department of Chemical and Environmental Engineering, Faculty of Engineering, Universiti Putra Malaysia, Serdang Selangor 43400, Malaysia

Corresponding author: Shameli Kamyar, kamyarshameli@gmail.com; parvaneh.shabanzade@gmail.com; kamyar@utm.my
Received Date: 10 November 2016
Revised Date: 3 January 2017
Accepted Date: 27 February 2017
Available Online: 28 July 2017

Figures(8)

A facile and green synthetic approach for fabrication of starch-stabilized magnetite nanoparticles was implemented at moderate temperature. This synthesis involved the use of iron salts, potato starch, sodium hydroxide and deionized water as iron precursors, stabilizer, reducing agent and solvent respectively. The nanoparticles (NPs) were characterized by UV-vis, PXRD, HR-TEM, FESEM, EDX, VSM and FT-IR spectroscopy. The ultrasonic assisted co-precipitation technique provides well formation of highly distributed starch/Fe₃O₄-NPs. Based on UV-vis analysis, the sample showed the characteristic of surface plasmon resonance in the presence of Fe₃O₄-NPs. The PXRD pattern depicted the characteristic of the cubic lattice structure of Fe₃O₄-NPs. HR-TEM analysis showed the good dispersion of NPs with a mean diameter and standard deviation of 10.68±4.207 nm. The d spacing measured from the lattice images were found to be around 0.30 nm and 0.52 nm attributed to the Fe₃O₄ and starch, respectively. FESEM analysis confirmed the formation of spherical starch/Fe₃O₄-NPs with the emission of elements of C, O and Fe by EDX analysis. The magnetic properties illustrated by VSM analysis indicated that the as synthesized sample has a saturation magnetization and coercivity of 5.30 emu/g and 22.898 G respectively. Additionally, the FTIR analysis confirmed the binding of starch with Fe₃O₄-NPs. This method was cost effective, facile and eco-friendly alternative for preparation of NPs.
- Nanoparticles,
- Fe₃O₄,
- Starch,
- Magnetic properties,
- Vibrating sample magnetometer
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