Citation: Li-E. Dong, Guo-Jing Gou, Xue-Qin Jin, Min Zhang. Synthesis pretreatment and characterization of a magnetic layered double hydroxides fluorescent probe[J]. Chinese Chemical Letters, ;2014, 25(6): 923-928. doi: 10.1016/j.cclet.2014.03.006 shu

Synthesis pretreatment and characterization of a magnetic layered double hydroxides fluorescent probe

1.
Medical Chemistry Department, School of Basic Medical, Ningxia Medical University, Yinchuan 750004, China

Corresponding author: Guo-Jing Gou,
Received Date: 5 January 2014
Available Online: 27 February 2014
Fund Project: This work was supported by the National Natural Science Foundation of China (Nos. 81260483, 20961008). (Nos. 81260483, 20961008)

Usingmagnetic layered double hydroxide (MLDH) as carrier of fluorescein (FLU), a fluorescent composite of MLDH-FLU was prepared via intercalation reaction of ion change. The crystal properties of MLDH-FLU were investigated through XRD, IR, TEM and TG-DSC characterization. It is shown that the crystal type of MLDH-FLU composite matched well with R-hexagonal crystal system of MLDH, with crystal cell parameters of a, c and channel height h equal to 0.3199, 2.411 and 0.3267 nm respectively. The superabundant pigment adsorbed outside the composite should be cleared before interference with cells, but excessive wash would decrease stability and cause crystal phase transformation of MLDH.
- Magnetic layered double hydroxides,
- Fluorescein,
- Intercalation,
- Dyeing mark
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沈阳化工大学材料科学与工程学院沈阳 110142