Citation: Ramin Rezaei Marzeih Karami. Microwave promoted rapid dehydration of aldoximes to nitrites using melamine-formaldehyde resin supported sulphuric acid in dry media[J]. Chinese Chemical Letters, ;2011, 22(7): 815-818. doi: 10.1016/j.cclet.2011.01.008
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A simple and convenient procedure for the synthesis of nitriles by dehydration of aldoxime using supported sulphuric acid on melamine-formaldehyde resin (MFR) under solvent-free condition has been developed. A variety of aromatic and aliphatic aldoximes were converted to the corresponding nitriles. The resin was recovered and reused for subsequent reactions.
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Keywords:
- Aldoximes,
- Nitriles,
- Melamine-formaldehyde resin,
- Sulphuric acid,
- Solvent-free
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