Citation: S. Allameh, M. M. Heravi, M. M. Hashemi, F. F. Bamoharram. Synthesis of 3-(aryl)-2-thioxo-2,3-dihydroquinazolin-4(1H)-one derivatives using heteropolyacids as green, heterogeneous and recyclable catalysts[J]. Chinese Chemical Letters, ;2011, 22(2): 131-134. doi: 10.1016/j.cclet.2010.10.012 shu

Synthesis of 3-(aryl)-2-thioxo-2,3-dihydroquinazolin-4(1H)-one derivatives using heteropolyacids as green, heterogeneous and recyclable catalysts

a Department of Chemistry, Science and Research Branch, Islamic Azad University, Tehran, Iran;
b Department of Chemistry, School of Sciences, Alzahra University, Vanak, Tehran, Iran;
c Department of Chemistry, Faculty of Sciences, Islamic Azad University, Mashhad Branch, Mashhad, Iran

Received Date: 31 May 2010

Reaction of isatoic anhydride with aniline derivatives gave 2-amino-N-(aryl) benzamides. The latters reacted with phenyli-sothiocyanate in the presence of heteropolyacids in various solvents which afforded 3-(aryl)-2-thioxo-2,3-dihydroquinazolin-4(1H)-one derivatives. The effects of various heteropolyacids including Preyssler and Keggin on the yields and reaction times have been investigated.
- Thioxo-quinazolinones,
- Recyclable catalysts,
- Heteropolyacids,
- Heterogeneous
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