Citation: Shadpour Mallakpour, Mehdi Hatami, Ali A. Ensafi, Hassan Karimi-Maleh. Synthesis and characterization of novel dopamine-derivative:Application of modified multi-wall carbon nanotubes paste electrode for electrochemical investigation[J]. Chinese Chemical Letters, ;2011, 22(2): 185-188. doi: 10.1016/j.cclet.2010.07.031 shu

Synthesis and characterization of novel dopamine-derivative:Application of modified multi-wall carbon nanotubes paste electrode for electrochemical investigation

Organic Polymer Chemistry Research Laboratory, Department of Chemistry, Isfahan University of Technology, Isfahan 84156-83111, Islamic Republic of Iran

Received Date: 28 May 2010

Fund Project: We wish to express our gratitude to the Research Affairs Division Isfahan University of Technology (IUT), Isfahan, for partial financial support. Further financial support from National Elite Foundation (NEF), Iran Nanotechnology Initiative Council (INIC) and Center of Excellency in Sensors and Green Chemistry Research (IUT) is gratefully acknowledged.

Novel dopamine-derivative compound, 3,5-diamino-N-(3,4-dihydroxyphenethyl)benzamide (3,5-DAB) was prepared in two steps. In the first step dopamine hydrochloride was reacted with 3,5-dinitrobenzoyl chloride in the presence of propylene oxide. In the second step reduction of nitro groups resulted in preparation of 3,5-DAB in quantitative yield. This material was characterized using conventional spectroscopic methods such as FT-IR and ¹H NMR. In addition, the redox response of a modified carbon nanotubes paste electrode of 3,5-DAB was investigated in aqueous solution at a neutral pH. The result showed that the electrode process has a guasi-reversible response, with △E_p, greater than the (59/n) mV expected for a reversible system. Finally, the diffusion coefficient for redox process in paraffin oil matrix obtained using chronoamperometry methods.
- 3,5-Diamino-N-(3,4-dihydroxyphenethyl)benzamide,
- Synthesis,
- Electrochemical investigation,
- Cyclic voltammetry,
- Multi-wall carbon nanotubes paste electrode
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