Citation: Lei Wang, Guang Ming Zhu. Synthesis and characterization of novel poly(aryl ether)s containing naphthyl moieties[J]. Chinese Chemical Letters, ;2009, 20(8): 965-968. doi: 10.1016/j.cclet.2009.02.019 shu

Synthesis and characterization of novel poly(aryl ether)s containing naphthyl moieties

Lei Wang ,
Guang Ming Zhu

Shenzhen Key Laboratory of Special Functional Materials and College of Materials Science and Engineering, Shenzhen University, Shenzhen 518060, China

Received Date: 8 December 2008

Fund Project: This project was financially supported by Natural Science Foundation of Guangdong Province (No.7301357) and Science and Technology Projects of Shenzhen City (No.200724).

Two poly(aryl ether)s containing naphthyl moieties were prepared from bis(3,5-dimethyl-4-hydroxyphenyl)naphthyl methane (monomer 1) via nucleophilic aromatic substitution polycondensation with bis(4-fluorophenyl) ketone and bis(4-fluorophenyl) sulfone. The structures of these polymers were confirmed by ¹H NMR. The M_n values of the two polymers were 96,200 and 88,600,respectively. The polymers exhibited good thermal stabilities with 5% mass loss at T>400℃ and high glass-transition temperature (T_g) of T>250℃. Moreover, the resultant polymers were amorphous determined by wide angle X-ray diffraction (WAXD).
- Poly(aryl ether)s,
- Naphthyl moieties,
- Thermal properties,
- Chemical synthesis
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