Citation: Ji Ming Xiang, Bao Lin Li. Solvent-free synthesis of some ethyl arylglyoxylates[J]. Chinese Chemical Letters, ;2009, 20(1): 55-57. doi: 10.1016/j.cclet.2008.10.003 shu

Solvent-free synthesis of some ethyl arylglyoxylates

Ji Ming Xiang ^a,b, ,
Bao Lin Li ^a

a School of Chemistry and Materials Science, and The Key Laboratory of Medicinal Plant Resource & Natural Pharmaceutical Chemistry of Ministry of Education, Shaanxi Normal University, Xi'an 710062, China;
b Department of Chemistry, Ankang University, Ankang 725000, China

Received Date: 7 July 2008

Fund Project: The authors are thankful to financial support from Science and Technology Key Project of Education Ministry, P.R. China (No: 105153) and Natural Science Foundation of Shaanxi Province, P.R. China (No. 2004B06).

An efficient and convenient approach to synthesize of ethyl arylglyoxylates by solvent-free grinding was described. Eight ethyl arylglyoxylates had been synthesized by this method, this method provided several advantages such as little pollution, high yield,good selectivity, and simple workup procedure, their structures were confirmed by IR, ¹HNMR.
- Ethyl arylglyoxylate,
- Friedel-Crafts acylation,
- Solvent-free reaction,
- Synthesis
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