Citation: Yi Ru Peng, Yu Hong Cao, Pei Feng Chen, Xiao Xia Huang. Synthesis of di-μ-oxo-tetra-(α-pentyloxy) tin(IV) phthalocyanine[J]. Chinese Chemical Letters, ;2008, 19(3): 273-276. doi: 10.1016/j.cclet.2007.12.020 shu

Synthesis of di-μ-oxo-tetra-(α-pentyloxy) tin(IV) phthalocyanine

College of Chemistry & Material Science, Fujian Normal University, Fuzhou 350007, China

Received Date: 24 September 2007

Fund Project: This study was supported by the National Natural Science Foundation of China (No. 20604007), Natural Science Foundation of Fujian (No. C0510007), Key Foundation for Ministry of Education, China (No. 206071), Key Foundation for Technology Department (2007I0013), Key Foundation for Education Office of Fujian (No. JA05195).

Axially substituted tin phthalocyanines, namely dichloride-tetra-(α-pentyloxy) tin (IV) phthalocyanine 2, dihydroxy-tetra-(α-pentyloxy) tin (IV) phthalocyanine 3 and its dimmer di-μ-oxo-tetra-(α-pentyloxy) tin (IV) phthalocyanine 4 were synthesized. The catalytic effect of H₂O-free CaCl₂ in quinoline was used for condensation of dihydroxy tin phthalocyanine 3 to the cofacially arraydimmer 4. Their structures were characterized by UV-vis, IR, elemental analysis, MS, as well as ¹HNMR spectroscopy.
- Axially substituted tin (IV) phthalocyanine,
- Dimmer,
- Synthesis,
- Characterization
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