无机-有机CdS/YBTPy S型光催化剂高效产氢及其机理

引用本文: 魏勉, 程畅, 何博文, 程蓓, 戚克振, 别传彪. 无机-有机CdS/YBTPy S型光催化剂高效产氢及其机理[J]. 物理化学学报, 2025, 41(12): 100158. doi: 10.1016/j.actphy.2025.100158 shu

Citation: Mian Wei, Chang Cheng, Bowen He, Bei Cheng, Kezhen Qi, Chuanbiao Bie. Inorganic-organic CdS/YBTPy S-scheme photocatalyst for efficient hydrogen production and its mechanism[J]. Acta Physico-Chimica Sinica, 2025, 41(12): 100158. doi: 10.1016/j.actphy.2025.100158 shu

无机-有机CdS/YBTPy S型光催化剂高效产氢及其机理

魏勉 ^{1, 2,} ,
程畅 ^3, ,
何博文 ^3, ,
程蓓 ^{1, 2,} ,
戚克振 ^{1,
,} ,
别传彪 ^{3,
,}

1.
大理大学药学院, 云南大理 671003
2.
武汉理工大学材料复合新技术全国重点实验室, 湖北武汉 430070
3.
中国地质大学(武汉), 材料与化学学院, 太阳燃料实验室, 湖北武汉 430078

通讯作者: 戚克振, qikezhen@dali.edu.cn; 别传彪, biechuanbiao@cug.edu.cn

基金项目:
国家重点研发计划 2022YFB3803600

国家自然科学基金 22202187

国家自然科学基金 U24A2071

国家自然科学基金 22278324

国家自然科学基金 22361142704

国家自然科学基金 22409181

国家自然科学基金 U23A20102

湖北省自然科学基金 2025AFB492

湖北省自然科学基金 2022CFA001

湖北省重点研发计划项目 2023BAB113

摘要: S型异质结因其优异的电荷分离能力和最大化的氧化还原电位，在高效光催化产氢领域受到广泛关注。本研究通过Yamamoto偶联反应合成新型芘-苯并噻二唑共轭聚合物(YBTPy)，并采用溶剂热法原位沉积CdS纳米颗粒，构建了CdS/YBTPy S型异质结光催化剂。优化后的CP5复合材料产氢速率达5.01 mmol h⁻¹ g⁻¹，较纯相CdS(1.20 mmol h⁻¹ g⁻¹)提升4.2倍。通过原位辐照X射线光电子能谱结合开尔文探针力显微镜，阐明了异质结界面的特征性S型电荷转移路径。此外，采用飞秒瞬态吸收光谱研究了光生载流子的动力学行为。该工作为有机-无机杂化S型光催化体系的设计提供了新的理论基础。

关键词:

English

Inorganic-organic CdS/YBTPy S-scheme photocatalyst for efficient hydrogen production and its mechanism

Mian Wei ^{1, 2,} ,
Chang Cheng ^3, ,
Bowen He ^3, ,
Bei Cheng ^{1, 2,} ,
Kezhen Qi ^{1,
,} ,
Chuanbiao Bie ^{3,
,}

1.
College of Pharmacy, Dali University, Dali 671003, Yunnan Province, China
2.
State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, Hubei Province, China
3.
Laboratory of Solar Fuel, Faculty of Materials Science and Chemistry, China University of Geosciences, Wuhan 430078, Hubei Province, China

Corresponding author: Email: qikezhen@dali.edu.cn (K.Z.); Email: biechuanbiao@cug.edu.cn (C.B.)

Received Date: 04 August 2025
Accepted Date: 14 August 2025
Revised Date: 12 August 2025
Available Online: 15 December 2025
Fund Project:
the financial support from the National Key Research and Development Program of China

the National Natural Science Foundation of China

the National Natural Science Foundation of China

the National Natural Science Foundation of China

the National Natural Science Foundation of China

the National Natural Science Foundation of China

the National Natural Science Foundation of China

the Hubei Provincial Natural Science Foundation of China

the Hubei Provincial Natural Science Foundation of China

the Key R & D Program Projects in Hubei Province

Abstract: S-scheme heterojunctions have garnered significant attention for efficient photocatalytic H₂ evolution due to their superior charge separation and maximized redox potential. In this study, we developed a novel pyrene-benzothiadiazole conjugated polymer (YBTPy) through Yamamoto coupling, followed by the in situ deposition of CdS nanoparticles via a solvothermal method to construct a CdS/YBTPy S-scheme heterojunction photocatalyst. The optimized composite, designated as CP5, demonstrated a hydrogen production rate of 5.01 mmol h⁻¹ g⁻¹, representing a 4.2-fold enhancement compared to pristine CdS (1.20 mmol h⁻¹ g⁻¹). The characteristic S-scheme charge transfer pathway at the heterojunction interface was elucidated using in situ irradiated X-ray photoelectron spectroscopy in conjunction with Kelvin probe force microscopy. Additionally, femtosecond transient absorption spectroscopy was employed to investigate the dynamics of photogenerated charge carriers. This work provides a new theoretical foundation for the design of organic–inorganic hybrid S-scheme photocatalytic systems.

Key words:

Conjugated polymers
/ S-scheme heterojunction
/ Photocatalytic hydrogen evolution
/ Femtosecond transient absorption spectroscopy

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1.
沈阳化工大学材料科学与工程学院沈阳 110142

无机-有机CdS/YBTPy S型光催化剂高效产氢及其机理

通讯作者: 戚克振, qikezhen@dali.edu.cn; 别传彪, biechuanbiao@cug.edu.cn

English

Inorganic-organic CdS/YBTPy S-scheme photocatalyst for efficient hydrogen production and its mechanism

Corresponding author: Email: qikezhen@dali.edu.cn (K.Z.); Email: biechuanbiao@cug.edu.cn (C.B.)

CCS Chemistry：嵌段共聚物自组装成 “三明治”二维有机材料，实现纳米级压力传感功能

CCS Chemistry：颜徐州、鲍哲南：你的皮肤可能是一片SPMs

CCS Chemistry：工作高效不疲劳，只须让催化剂动起来

CCS Chemistry：静电组装导向聚合- 聚电解质纳米凝胶量化制备新策略

CCS Chemistry：金黄色葡萄球菌醛基脱氢酶是如何识别特异性底物的？

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通讯作者: 陈斌, bchen63@163.com

中国化学会秘书处

无机-有机CdS/YBTPy S型光催化剂高效产氢及其机理

通讯作者: 戚克振, qikezhen@dali.edu.cn; 别传彪, biechuanbiao@cug.edu.cn

English

Inorganic-organic CdS/YBTPy S-scheme photocatalyst for efficient hydrogen production and its mechanism

Corresponding author: Email: qikezhen@dali.edu.cn (K.Z.); Email: biechuanbiao@cug.edu.cn (C.B.)

CCS Chemistry：嵌段共聚物自组装成 “三明治”二维有机材料，实现纳米级压力传感功能

CCS Chemistry：颜徐州、鲍哲南： 你的皮肤可能是一片SPMs

CCS Chemistry：工作高效不疲劳，只须让催化剂动起来

CCS Chemistry：静电组装导向聚合- 聚电解质纳米凝胶量化制备新策略

CCS Chemistry：金黄色葡萄球菌醛基脱氢酶是如何识别特异性底物的？

计量

文章相关

通讯作者: 陈斌, bchen63@163.com

中国化学会秘书处

CCS Chemistry：颜徐州、鲍哲南：你的皮肤可能是一片SPMs