Citation: Jiaqi Yang, Xuqiang Hao, Jiejie Jing, Yuqiang Hao, Zhiliang Jin. 3D/2D ReSe₂/ZnCdS S-scheme photocatalyst with efficient interfacial charge separation for optimized hydrogen production[J]. Acta Physico-Chimica Sinica, ;2025, 41(10): 100131. doi: 10.1016/j.actphy.2025.100131 shu

3D/2D ReSe₂/ZnCdS S-scheme photocatalyst with efficient interfacial charge separation for optimized hydrogen production

Jiaqi Yang ^{1, 2} ,
Xuqiang Hao ^{1, 2,,} ,
Jiejie Jing ^{1, 2} ,
Yuqiang Hao ^{1, 2} ,
Zhiliang Jin ^{1, 2}

1.
School of Chemistry and Chemical Engineering, North Minzu University, Yinchuan 750021, Ningxia Hui Autonomous Region, China
2.
Ningxia Key Laboratory of Solar Chemical Conversion Technology, Key Laboratory for Chemical Engineering and Technology, State Ethnic Affairs Commission, North Minzu University, Yinchuan 750021, Ningxia Hui Autonomous Region, China

Corresponding author: Xuqiang Hao, haoxuqiang@nun.edu.cn
Received Date: 18 June 2025
Revised Date: 17 July 2025
Accepted Date: 18 July 2025

Fund Project: Ningxia Hui Autonomous Region full-time introduced high-level talent research project 2023BSB03047

The rational construction of step-scheme (S-scheme) heterojunctions has been demonstrated as an effective strategy to optimize interfacial charge carrier separation dynamics in semiconductor photocatalysts. In this work, a hierarchical ReSe₂/ZnCdS S-scheme heterojunction with well-defined architectures was successfully synthesized via an ultrasonication-assisted synthetic strategy, achieving precise nanostructure control and enhanced interfacial coupling for optimized photogenerated charge dynamics. The disordered nanoflower-like ReSe₂ architecture enhances light-harvesting efficiency and the density of surface reaction sites, and significantly suppresses ZnCdS nanoparticle aggregation. The optimized 5%ReSe₂/ZnCdS composite exhibits an exceptional hydrogen evolution rate of 13.96 mmol∙g⁻¹∙h⁻¹ under visible light irradiation, representing a 5.91-fold enhancement over pristine ZnCdS (2.36 mmol∙g⁻¹∙h⁻¹) and outperforming most conventional heterojunction systems. The outstanding photocatalytic performance is attributed to the formation of the ReSe₂/ZnCdS S-scheme heterojunction, which promotes the separation of photogenerated electrons and holes, enhancing the photo-redox capacity. Combining in situ X-ray photoelectron spectroscopy (XPS) analysis and density functional theory (DFT) calculations further conform the S-scheme charge transfer mechanism at the heterointerface of ReSe₂/ZnCdS. Furthermore, Gibbs free energy calculations of hydrogen adsorption confirm that ReSe₂ as the predominant catalytic center provides more favorable hydrogen adsorption kinetics than ZnCdS. This work provides a universal framework to design ZnCdS-based S-scheme heterojunctions for high-efficiency photocatalytic hydrogen evolution.
- S-scheme,
- Photocatalytic hydrogen evolution,
- ZnCdS,
- ReSe₂,
- Internal electric field
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沈阳化工大学材料科学与工程学院沈阳 110142

3D/2D ReSe2/ZnCdS S-scheme photocatalyst with efficient interfacial charge separation for optimized hydrogen production

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通讯作者: 陈斌, bchen63@163.com

3D/2D ReSe₂/ZnCdS S-scheme photocatalyst with efficient interfacial charge separation for optimized hydrogen production