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Citation: Menglan Wei, Xiaoxia Ou, Yimeng Wang, Mengyuan Zhang, Fei Teng, Kaixuan Wang. S-scheme heterojunction g-C3N4/Bi2WO6 highly efficient degradation of levofloxacin: performance, mechanism and degradation pathway[J]. Acta Physico-Chimica Sinica, ;2025, 41(9): 100105. doi: 10.1016/j.actphy.2025.100105 shu

S-scheme heterojunction g-C3N4/Bi2WO6 highly efficient degradation of levofloxacin: performance, mechanism and degradation pathway

  • College of Environment and Resources, Dalian Minzu University, Dalian 116600, Liaoning Province, China

  • Corresponding author: Xiaoxia Ou, ouxiaoxia@dlnu.edu.cn
  • Received Date: 5 March 2025
    Revised Date: 9 May 2025
    Accepted Date: 12 May 2025

    Fund Project: the Liaoning Provincial Science and Technology Program Joint Plan 2023JH2/101800001the Basic Scientific Research Fund of Liaoning Provincial Education Department LJKMZ20220396Dalian Science and Technology Talents Innovation Support Program 2024RQ056

  • g-C3N4/Bi2WO6 (MCN/BWO) heterojunction photocatalysts were synthesized via a one-step hydrothermal method for the degradation of levofloxacin (LEV). Under simulated sunlight irradiation, the degradation rate of LEV by MCN/BWO with a molar ratio of 1 : 1 reached 98.14%, which was attributed to the formation of an S-scheme heterojunction between MCN and BWO. In situ XPS analysis and surface work function measurements confirmed that the electron transfer pathway follows the S-scheme heterojunction mechanism. The internal electric field (IEF) generated by the S-scheme heterojunction in the MCN/BWO system facilitates direct transfer of photogenerated electrons (e−) from the conduction band (CB) of BWO to the valence band (VB) of MCN. This process enables efficient separation of photogenerated electron-hole (e−-h+) pairs, with h⁺ accumulating on the VB of BWO and e− accumulating on the CB of MCN. Free radical trapping experiments demonstrated that the superoxide free radical (·O₂−) and h⁺ were the primary active species. Besides exhibiting superior photocatalytic performance, the catalyst maintained excellent stability over three consecutive cycles. To elucidate the degradation mechanism, liquid chromatography-mass spectrometry (LC-MS) and quantitative structure-activity relationship (QSAR) analysis were employed to identify degradation pathways, intermediates, and potential toxicity. This study provides a theoretical foundation for wastewater treatment applications.
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