Citation: Jiajie Cai, Chang Cheng, Bowen Liu, Jianjun Zhang, Chuanjia Jiang, Bei Cheng. CdS/DBTSO-BDTO S型异质结光催化制氢及其电荷转移动力学[J]. Acta Physico-Chimica Sinica, ;2025, 41(8): 100084. doi: 10.1016/j.actphy.2025.100084 shu

CdS/DBTSO-BDTO S型异质结光催化制氢及其电荷转移动力学

1.
State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, Hubei Province, China;
2.
Laboratory of Solar Fuel, Faculty of Materials Science and Chemistry, China University of Geosciences, Wuhan 430078, Hubei Province, China;
3.
College of Environmental Science and Engineering, Nankai University, Tianjin 300350, China

Received Date: 20 February 2025
Revised Date: 10 March 2025
Accepted Date: 24 March 2025

Fund Project: This work was supported by the National Key Research and Development Program of China (2022YFB3803600), the National Natural Science Foundation of China (22238009, 22361142704, 22261142666, 22278324, 52073223), the Natural Science Foundation of Hubei Province of China (2022CFA001), and the Fundamental Research Funds for the Central Universities (63241632).

光催化分解水产氢具有广阔的应用前景。然而，单一光催化剂由于光生电子与空穴易复合，导致光催化产氢效率较低，严重制约了该技术的实际应用。构建异质结是克服这些缺点的有效策略，最近S型异质结脱颖而出，显示出了高效的促进电子和空穴分离的能力，同时最大限度地提高光催化剂的氧化还原能力。其中，基于聚合物的S型光催化剂正在兴起，但无机-有机S型异质结中的载流子动力学仍有待阐明。在本工作中，我们制备了由共轭聚合物双氧硫芴苯并二噻吩二酮(dibenzothiophene-S,S-dioxide-alt-benzodithiophene, DBTSO-BDTO)和硫化镉(CdS)组成的S型异质结，并研究了其光催化制氢的性能和界面电荷传输机制。利用原位辐照X射线光电子能谱验证了S型电子转移机理，并利用飞秒瞬态吸收光谱深入分析了S型异质结中载流子的动力学，证实有大量光生电子发生了界面电荷转移。由于S型异质结对载流子效率的提高和氧化还原能力的增强，复合材料的性能超过了DBTSO-BDTO和CdS，并且最优化复合材料的析氢速率达到3313 μmol·h^-1·g^-1，约为纯CdS的3倍。本工作为S型异质结的电子转移机制提供了新的视角，并可指导用于太阳能燃料生产的聚合物基光催化剂的开发。
- Photocatalysis,
- Cadmium sulfide,
- S-scheme heterojunction,
- H₂ production,
- Femtosecond transient absorption spectroscopy
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沈阳化工大学材料科学与工程学院沈阳 110142