Citation: Mingjie Lei, Wenting Hu, Kexin Lin, Xiujuan Sun, Haoshen Zhang, Ye Qian, Tongyue Kang, Xiulin Wu, Hailong Liao, Yuan Pan, Yuwei Zhang, Diye Wei, Ping Gao. Co/Mn/Mo掺杂加速NiSe₂重构以提高其电催化尿素氧化性能[J]. Acta Physico-Chimica Sinica, ;2025, 41(8): 100083. doi: 10.1016/j.actphy.2025.100083 shu

Co/Mn/Mo掺杂加速NiSe₂重构以提高其电催化尿素氧化性能

Mingjie Lei ¹ ,
Wenting Hu ² ,
Kexin Lin ¹ ,
Xiujuan Sun ¹ ,
Haoshen Zhang ¹ ,
Ye Qian ¹ ,
Tongyue Kang ¹ ,
Xiulin Wu ¹ ,
Hailong Liao ¹ ,
Yuan Pan ¹ ,
Yuwei Zhang ² ,
Diye Wei ¹ ,
Ping Gao ¹

1.
Key Laboratory of Environmentally Friendly Chemistry and Applications of Ministry of Education, College of Chemistry, Xiangtan University, Xiangtan 411105, Hunan Province, China;
2.
GDMPA Key Laboratory for Process Control and Quality Evaluation of Chiral Pharmaceuticals, Guangzhou Key Laboratory of Analytical Chemistry for Biomedicine, School of Chemistry, South China Normal University, Guangzhou 510006, Guangdong Province, China

Received Date: 21 January 2025
Revised Date: 8 March 2025
Accepted Date: 23 March 2025

Fund Project: The project was supported by the Scientific Research Fund of Hunan Provincial Education Department (23B0114), the Natural Science Foundation of Hunan Province (2024JJ5368), the National Natural Science Foundation of China (22122402), and the Natural Science Foundation of Guangdong Province (2021B1515020048).

尿素氧化反应(UOR)是一种很有前途的可再生能源生产技术，为电解水制氢提供了有效的替代方案，因此开发高效稳定的UOR催化剂至关重要。本文通过NaBH₄还原和硒化策略合成了富含Co、Mn和Mo的硒化镍催化剂(NiCoMnMo-Se)，该催化剂具有球形纳米颗粒与纳米片共存结构。X射线光电子能谱(XPS)、紫外-可见分光光度法(UV-vis)和原位bode相图表明，Mn和Mo的协同效应调节了Ni/Co的电子结构，提高了硒化物的电导率并加速加速电荷转移动力学，从而促进Ni²⁺/Co²⁺快速转变为活性Ni³⁺/Co³⁺，并显著降低了NiCoMnMo-Se的起始电位。在UOR过程中，大部分Mo和Se被氧化成钼酸盐和硒酸盐溶解在电解质中，暴露出更多的Ni(Co)OOH活性位点，从而加快UOR反应。另外，Mn的引入稳固了活性位点，极大地增强催化剂的整体稳定性。正如预期的那样，NiCoMnMo-Se催化剂在UOR过程中表现出优异的电催化和稳定性性能，在仅1.38 V vs. RHE (相对于可逆氢电极)的电位下实现了50 mA·cm^-2的电流密度，并在50 mA·cm^-2电流密度下运行50 h后电压仅上升3.0%。当NiCoMnMo-Se和商业Pt/C组装成用于碱性尿素电解的双电极体系时，它只需要1.59 V vs. RHE便达到50 mA·cm^-2。
- Urea oxidation reaction,
- Hydrogen production,
- NiCoMnMo-Se,
- Synergetic effect,
- Urea electrolysis,
- Ni-based selenide
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Co/Mn/Mo掺杂加速NiSe2重构以提高其电催化尿素氧化性能

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Co/Mn/Mo掺杂加速NiSe₂重构以提高其电催化尿素氧化性能