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Citation: Hassan Kefayati, Mostafa Golshekan, Shahab Shariati, Mahsa Bagheri. Fe3O4@MCM-48-SO3H: An efficient magnetically separable nanocatalyst for the synthesis of benzo[f]chromeno[2, 3-d]pyrimidinones[J]. Chinese Journal of Catalysis, ;2015, 36(4): 572-578. doi: 10.1016/S1872-2067(14)60286-2 shu

Fe3O4@MCM-48-SO3H: An efficient magnetically separable nanocatalyst for the synthesis of benzo[f]chromeno[2, 3-d]pyrimidinones

  • 1.

    a Department of Chemistry, Rasht Branch, Islamic Azad University, Rasht, Iran;

  • Corresponding author: Hassan Kefayati, 
  • Received Date: 23 October 2014
    Available Online: 6 January 2015

    Fund Project:

  • Sulfonic acid groups were grafted onto three different types of synthesized magnetic nanoparticles, namely Fe3O4, Fe3O4@SiO2, and Fe3O4@MCM-48. The sulfonic acid-functionalized nanoparticles were evaluated as catalysts for the synthesis of 5-aryl-1H-benzo[f]chromeno[2,3-d]pyrimidine- 2,4(3H,5H)-dione derivatives in terms of activity and recyclability. Their catalytic activities were compared with that of the homogeneous acid catalyst 1-methylimidazolium hydrogen sulfate ([HMIm][HSO4]). The activity of Fe3O4@MCM-48-SO3H was comparable to those of the other heterogeneous and homogeneous catalysts.
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