Citation: Chao Su, Song-Mei Ma, Geng-Xin Liu, Shu-Guang Yang. Dewetting Behavior of Hydrogen Bonded Polymer Complex Film under Hydrothermal Condition[J]. Chinese Journal of Polymer Science, ;2018, 36(9): 1036-1042. doi: 10.1007/s10118-018-2109-8 shu

Dewetting Behavior of Hydrogen Bonded Polymer Complex Film under Hydrothermal Condition

a.
State Key Laboratory for Modification of Chemical Fibers and Polymer Materials, Center for Advanced Low-dimension Materials, College of Material Science and Engineering, Donghua University, Shanghai 201620, China
b.
Department of Polymer Science, The University of Akron, OH 44325, USA

Corresponding author: Shu-Guang Yang, shgyang@dhu.edu.cn
Received Date: 13 December 2017
Revised Date: 4 January 2018
Accepted Date: 10 January 2018
Available Online: 15 March 2018

Hydrogen-bonded polymer complex films with the thickness ranging from 50 nm to 2400 nm were prepared by layer-by-layer (LbL) assembly of poly(2-ethyl-2-oxazoline) (PEOX) and poly(acrylic acid) (PAA). The dewetting behavior of PEOX/PAA films under hydrothermal condition was investigated. It was found that the dewetting occurred at solid-liquid interface, and the typical morphologies such as holes, irregular cellular structure, and droplets were observed. Atomic force microscopy (AFM) revealed the initial rupture of the film. Microscopic Raman and infrared (IR) imaging demonstrated that the PEOX and PAA chains remained association during the dewetting process.
- Hydrogen-bonding,
- Polymer complex,
- Dewetting
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