具有光热效应的多级Ti3C2/Bi12O17Br2肖特基异质结简单合成及其太阳能驱动抗生素光降解的研究

引用本文: 刘超, 余欢, 李佳明, 余茜, 郁壮志, 宋玉玺, 张峰, 张勤芳, 邹志刚. 具有光热效应的多级Ti₃C₂/Bi₁₂O₁₇Br₂肖特基异质结简单合成及其太阳能驱动抗生素光降解的研究[J]. 物理化学学报, 2025, 41(7): 100075. doi: 10.1016/j.actphy.2025.100075 shu

Citation: Chao Liu, Huan Yu, Jiaming Li, Xi Yu, Zhuangzhi Yu, Yuxi Song, Feng Zhang, Qinfang Zhang, Zhigang Zou. 具有光热效应的多级Ti₃C₂/Bi₁₂O₁₇Br₂肖特基异质结简单合成及其太阳能驱动抗生素光降解的研究[J]. Acta Physico-Chimica Sinica, 2025, 41(7): 100075. doi: 10.1016/j.actphy.2025.100075 shu

具有光热效应的多级Ti₃C₂/Bi₁₂O₁₇Br₂肖特基异质结简单合成及其太阳能驱动抗生素光降解的研究

刘超 ^{1,
,} ,
余欢 ^1, ,
李佳明 ^1, ,
余茜 ^1, ,
郁壮志 ^1, ,
宋玉玺 ^1, ,
张峰 ^1, ,
张勤芳 ^{1,
,} ,
邹志刚 ^2,

1.
盐城工学院材料科学与工程学院, 江苏盐城 224051
2.
南京大学生态材料与可再生能源研究中心, 江苏南京 210093

通讯作者: 刘超, cliu@ycit.edu.cn; 张勤芳, qfangzhang@ycit.edu.cn

基金项目:
国家自然科学基金 12474276

国家自然科学基金 12274361

江苏高校青蓝工程资助项目

摘要: 在去除盐酸四环素(TC)方面，光催化技术被认为是一种高效和绿色的方法，可满足可持续发展的需求。本研究采用简单的搅拌过程来构建具有多级结构的Ti₃C₂/Bi₁₂O₁₇Br₂ (命名为TBOB)肖特基异质结，其中Bi₁₂O₁₇Br₂组分紧密地沉积在Ti₃C₂表面。通过模拟太阳光下降解TC来评价所有样品的光催化性能。与Bi₁₂O₁₇Br₂相比，所制备的TBOB复合材料表现出更好的光降解活性，活性的增强归功于Ti₃C₂和Bi₁₂O₁₇Br₂之间的协同效应，增加Ti₃C₂的负载量可提高光捕获能力，肖特基异质结的形成可促进有效的电荷载流子分离，以及光热效应可促进表面反应动力学。此外，对影响TBOB复合材料光催化性能的关键因素进行了详细的研究。自由基捕获实验和电子顺磁共振(EPR)技术证实了•O₂⁻和e⁻是TC光催化降解的主要活性物种。结合实验分析和理论计算，提出并讨论了可能的电荷载流子转移途径和光催化降解机理。本研究为合理设计高效光热辅助Ti₃C₂基光催化剂提供了理论和实验依据。

关键词:

English

具有光热效应的多级Ti₃C₂/Bi₁₂O₁₇Br₂肖特基异质结简单合成及其太阳能驱动抗生素光降解的研究

Chao Liu ^{1,
,} ,
Huan Yu ^1, ,
Jiaming Li ^1, ,
Xi Yu ^1, ,
Zhuangzhi Yu ^1, ,
Yuxi Song ^1, ,
Feng Zhang ^1, ,
Qinfang Zhang ^{1,
,} ,
Zhigang Zou ^2,

1.
School of Materials Science and Engineering, Yancheng Institute of Technology, Yancheng 224051, Jiangsu Province, China
2.
Eco-Materials and Renewable Energy Research Centre (ERERC), Nanjing University, Nanjing 210093, Jiangsu Province, China

Corresponding author: Email: cliu@ycit.edu.cn (C.L.); Email: qfangzhang@ycit.edu.cn (Q.Z.)

Received Date: 17 January 2025
Accepted Date: 03 March 2025
Revised Date: 24 February 2025
Available Online: 15 July 2025
Fund Project:
the National Natural Science Foundation of Chin

the National Natural Science Foundation of Chin

Qinglan Project of Jiangsu of China

Abstract: 在去除盐酸四环素(TC)方面，光催化技术被认为是一种高效和绿色的方法，可满足可持续发展的需求。本研究采用简单的搅拌过程来构建具有多级结构的Ti₃C₂/Bi₁₂O₁₇Br₂ (命名为TBOB)肖特基异质结，其中Bi₁₂O₁₇Br₂组分紧密地沉积在Ti₃C₂表面。通过模拟太阳光下降解TC来评价所有样品的光催化性能。与Bi₁₂O₁₇Br₂相比，所制备的TBOB复合材料表现出更好的光降解活性，活性的增强归功于Ti₃C₂和Bi₁₂O₁₇Br₂之间的协同效应，增加Ti₃C₂的负载量可提高光捕获能力，肖特基异质结的形成可促进有效的电荷载流子分离，以及光热效应可促进表面反应动力学。此外，对影响TBOB复合材料光催化性能的关键因素进行了详细的研究。自由基捕获实验和电子顺磁共振(EPR)技术证实了•O₂⁻和e⁻是TC光催化降解的主要活性物种。结合实验分析和理论计算，提出并讨论了可能的电荷载流子转移途径和光催化降解机理。本研究为合理设计高效光热辅助Ti₃C₂基光催化剂提供了理论和实验依据。

Key words:

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沈阳化工大学材料科学与工程学院沈阳 110142

具有光热效应的多级Ti₃C₂/Bi₁₂O₁₇Br₂肖特基异质结简单合成及其太阳能驱动抗生素光降解的研究

通讯作者: 刘超, cliu@ycit.edu.cn; 张勤芳, qfangzhang@ycit.edu.cn

English

具有光热效应的多级Ti₃C₂/Bi₁₂O₁₇Br₂肖特基异质结简单合成及其太阳能驱动抗生素光降解的研究

Corresponding author: Email: cliu@ycit.edu.cn (C.L.); Email: qfangzhang@ycit.edu.cn (Q.Z.)

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