引用本文:
Dun Qing WANG, Dai Rong CHEN, Xiu Ling JIAO. Synthesis of Nickel Sulfide Particles by Solvothermal Process[J]. Chinese Chemical Letters,
2004, 15(1): 79-82.
Citation: Dun Qing WANG, Dai Rong CHEN, Xiu Ling JIAO. Synthesis of Nickel Sulfide Particles by Solvothermal Process[J]. Chinese Chemical Letters, 2004, 15(1): 79-82.
Citation: Dun Qing WANG, Dai Rong CHEN, Xiu Ling JIAO. Synthesis of Nickel Sulfide Particles by Solvothermal Process[J]. Chinese Chemical Letters, 2004, 15(1): 79-82.
Synthesis of Nickel Sulfide Particles by Solvothermal Process
摘要:
Pyrite nickel disulfide and millerite nickel monosulfide have been successfully prepared by solvothermal method based on the reaction of Ni(NO3)2·6H2O and H2NC(S)NH2 in benzene and ethylenediamine (EDA). The final products were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM). The effects of the solvent, reaction temperature and time on the morphology and phase of the products have been discussed.
English
Synthesis of Nickel Sulfide Particles by Solvothermal Process
Abstract:
Pyrite nickel disulfide and millerite nickel monosulfide have been successfully prepared by solvothermal method based on the reaction of Ni(NO3)2·6H2O and H2NC(S)NH2 in benzene and ethylenediamine (EDA). The final products were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM). The effects of the solvent, reaction temperature and time on the morphology and phase of the products have been discussed.
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Key words:
- Chalcogenides
- / solvothermal synthesis
- / X-ray diffraction analysis
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