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由喹喔啉类配体构筑的钴的配合物的水热合成及晶体结构

黄艳菊 ,  倪良 ,  仝博 ,  邢伟男

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引用本文: 黄艳菊, 倪良, 仝博, 邢伟男. 由喹喔啉类配体构筑的钴的配合物的水热合成及晶体结构[J]. 无机化学学报, 2013, 29(6): 1289-1294. doi: 10.3969/j.issn.1001-4861.2013.00.221 shu
Citation:  HUANG Yan-Ju, NI Liang, TONG Bo, XING Wei-Nan. Hydrothermal Synthesis and Crystal Structure of a Cobalt Coordination Compound with Quinoxaline-Type Ligand[J]. Chinese Journal of Inorganic Chemistry, 2013, 29(6): 1289-1294. doi: 10.3969/j.issn.1001-4861.2013.00.221 shu

由喹喔啉类配体构筑的钴的配合物的水热合成及晶体结构

摘要: 采用水热法合成了一个配合物[Co(AIP)(HAIP)2]·(OH)2(HAIP=2-(9-anthryl)-1H-imidazo[4,5-f][1,10] phenanthroline)1,并对其进行了元素分析、红外光谱、热重表征和X射线单晶衍射测定。配合物1属于单斜晶系,空间群为C2/c,晶胞参数为:a=1.152 9(2),b=3.673 6(7),c=1.584 1(3) nm,α=107.73(3)°,V=6.382(2) nm3,Z=4(291(2) K)。在晶体中,中心离子Co(Ⅲ)分别与来自于2个不同的HAIP配体和1个AIP配体上的6个氮原子形成六配位的变形八面体构型。

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  • 收稿日期:  2012-07-21
  • 网络出版日期:  2013-03-04
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