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介孔氧化镍的复合表面活性剂模版法制备及表征

袁伟 ,  刘昉 ,  张昭

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引用本文: 袁伟, 刘昉, 张昭. 介孔氧化镍的复合表面活性剂模版法制备及表征[J]. 无机化学学报, 2013, 29(4): 803-809. doi: 10.3969/j.issn.1001-4861.2013.00.052 shu
Citation:  YUAN Wei, LIU Fang, ZHANG Zhao. Preparation and Characterization of Mesoporous Nickel Oxide Templated by Different Mixed Surfactants[J]. Chinese Journal of Inorganic Chemistry, 2013, 29(4): 803-809. doi: 10.3969/j.issn.1001-4861.2013.00.052 shu

介孔氧化镍的复合表面活性剂模版法制备及表征

  • 基金项目:

    国家自然科学基金(No.51004074)资助项目。 (No.51004074)

摘要: 用六水合硝酸镍为镍源, 尿素为沉淀剂, 以少量的复合表面活性剂(SDS/P123, CTAB/P123, CTBA/SDS)为模板水热制备了介孔氧化镍。分别采用热重-差示扫描量热(TG-DSC)、傅立叶红外光谱(FTIR)、X射线衍射(XRD)、氮气吸附脱附、扫描电子显微镜(SEM)、透射电子显微镜(TEM)对产物的结构和形貌进行了表征。用循环伏安法, 恒电流充放电和交流阻抗谱等对材料进行了电化学性能的测试。结果表明, 以复合表面活性剂SDS/P123为模板制备的介孔氧化镍有最大的比表面积、孔径和比电容, 且当SDS/P123质量比为2:1时, 所制备的氧化镍比表面积、孔径和比电容分别为209 m2·g-1, 0.407 cm3·g-1, 265 F·g-1。

English

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  • 收稿日期:  2012-08-28
  • 网络出版日期:  2012-10-30
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