引用本文:
张晟卯, 张治军, 党鸿辛, 刘维民, 薛群基. TiO2/聚丙烯酸丁酯纳米复合薄膜的制备及结构表征[J]. 物理化学学报,
2003, 19(02): 171-173.
doi:
10.3866/PKU.WHXB20030217
Citation: Zhang Sheng-Mao, Zhang Zhi-Jun, Dang Hong-Xin, Liu Wei-Min, Xue Qun-Ji. Preparation and Characterization of TiO2/Poly(butyl acrylate) Nanocomposite Film[J]. Acta Physico-Chimica Sinica, 2003, 19(02): 171-173. doi: 10.3866/PKU.WHXB20030217
Citation: Zhang Sheng-Mao, Zhang Zhi-Jun, Dang Hong-Xin, Liu Wei-Min, Xue Qun-Ji. Preparation and Characterization of TiO2/Poly(butyl acrylate) Nanocomposite Film[J]. Acta Physico-Chimica Sinica, 2003, 19(02): 171-173. doi: 10.3866/PKU.WHXB20030217
TiO2/聚丙烯酸丁酯纳米复合薄膜的制备及结构表征
摘要:
利用微乳液原位聚合法在普通玻璃表面上制备了TiO2/聚丙烯酸丁酯纳米复合膜.采用傅立叶变换红外光谱、高分辨透射电子显微镜和X射线光电子能谱对膜的结构进行了表征.结果表明， TiO2以纳米线的形式弥散在聚丙烯酸丁酯的高分子网络中，并且所制备的TiO2纳米线具有板钛矿相结构.
English
Preparation and Characterization of TiO2/Poly(butyl acrylate) Nanocomposite Film
Abstract:
The nano-TiO2/Poly(butyl acrylate) composite film was prepared by microemulsion in-situ polymerization method on glass substrate. The structure of the thin film was characterized by FTIR, XPS and HRTEM (high-resolution TEM) techniques. The results of FTIR analyses indicated that the poly(butyl acrylate) networks formed through in-situ polymerization. XPS results showed that Ti(OC4H9)4 changed into TiO2 through hydrolyzation. HRTEM of polymerized thin film indicated that the TiO2 nanolines are dispersed in the poly(butyl acrylate) networks.
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