引用本文:
刘佐才, 崔秀山, 范广裕, 邓百鸣, 王焕忠, 李云政. 1-甲基-3-吲哚甲叉(异丙叉)琥珀酸酐(I)和1-甲基-3-吲哚乙叉(异丙叉)琥珀酸酐(II)的晶体结构[J]. 物理化学学报,
1990, 6(02): 224-228.
doi:
10.3866/PKU.WHXB19900218
Citation: Liu Zuo-Cai, Cui Xiu-Shan, Fan Guang-Yu, Deng Bai-Ming, Wang Huan-Zhong, Li Yun-Zheng. Crystal Structures of 1-Methyl-3-Indolmethy-Lidene (Isopropylidene) Succinic Anhydride (I) and 1-Methyl-3-Indolethylidene (Isopropylidene) Succinic Anhydride(II)[J]. Acta Physico-Chimica Sinica, 1990, 6(02): 224-228. doi: 10.3866/PKU.WHXB19900218

Citation: Liu Zuo-Cai, Cui Xiu-Shan, Fan Guang-Yu, Deng Bai-Ming, Wang Huan-Zhong, Li Yun-Zheng. Crystal Structures of 1-Methyl-3-Indolmethy-Lidene (Isopropylidene) Succinic Anhydride (I) and 1-Methyl-3-Indolethylidene (Isopropylidene) Succinic Anhydride(II)[J]. Acta Physico-Chimica Sinica, 1990, 6(02): 224-228. doi: 10.3866/PKU.WHXB19900218

1-甲基-3-吲哚甲叉(异丙叉)琥珀酸酐(I)和1-甲基-3-吲哚乙叉(异丙叉)琥珀酸酐(II)的晶体结构
English
Crystal Structures of 1-Methyl-3-Indolmethy-Lidene (Isopropylidene) Succinic Anhydride (I) and 1-Methyl-3-Indolethylidene (Isopropylidene) Succinic Anhydride(II)
Abstract:
The crystal structures of the title compound (Ⅰ) and (Ⅱ) have been determined by X-ray diffraction. Crystal data are: C_(17)H_(15)NO_3(Ⅰ), triclinic, α=0.7308(2) nm, b=0.8845(3) nm, c=1.1323(3) nm, α=100.03(2)°, β=104.81(2)°, γ=97.20(2)°, V=0.6856(3) nm, Z=2, R=0.047 and C_(18)H_(17)NO_3(Ⅱ), monoclinic, a=1.1006(3) nm, b=1.1172(2) nm, c=1.4046(3) nm, β=102.78(2)°, V=1.5337(6) nm, Z=4, R=0.055. The molecular conformation is cis form for compound Ⅰ and trans form for compound(Ⅱ).

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