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A voltammetric sensor with a multiwall carbon nanotube paste electrode and naphthol green as a mediator for the determination of N-actylcysteine in the presence of tryptophan

Mohsen Keyvanfard ,  Maryam Tahmasbi ,  Hassan Karimi-Maleh ,  Khadijeh Alizad

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引用本文: Mohsen Keyvanfard, Maryam Tahmasbi, Hassan Karimi-Maleh, Khadijeh Alizad. A voltammetric sensor with a multiwall carbon nanotube paste electrode and naphthol green as a mediator for the determination of N-actylcysteine in the presence of tryptophan[J]. 催化学报, 2014, 35(4): 501-508. doi: 10.1016/S1872-2067(14)60019-X shu
Citation:  Mohsen Keyvanfard, Maryam Tahmasbi, Hassan Karimi-Maleh, Khadijeh Alizad. A voltammetric sensor with a multiwall carbon nanotube paste electrode and naphthol green as a mediator for the determination of N-actylcysteine in the presence of tryptophan[J]. Chinese Journal of Catalysis, 2014, 35(4): 501-508. doi: 10.1016/S1872-2067(14)60019-X shu

A voltammetric sensor with a multiwall carbon nanotube paste electrode and naphthol green as a mediator for the determination of N-actylcysteine in the presence of tryptophan

    通讯作者: Mohsen Keyvanfard, Hassan Karimi-Maleh; Mohsen Keyvanfard, Hassan Karimi-Maleh
摘要: A multiwall carbon nanotube modified electrode prepared by incorporating multiwall carbon nanotubes in the electrode of a sensor and naphthol green as a homogeneous mediator was used as a voltammetric sensor for the determination of N-actylcysteine (N-AC) in the presence of tryptophan (Trp). The voltammograms of differential pulse voltammetry of N-AC in a mixture with Trp were separated from each other by a potential difference of 200 mV, which allowed the determination of both N-AC and Trp simultaneously. Under the optimum conditions, the electrocatalytic currents increased linearly with N-AC concentration in the range of 0.25-400 μmol/L (two linear segments with different slopes). The detection limit for N-AC was 0.08 μmol/L. The kinetic parameters of the system were determined using electrochemical methods. The method was applied for the determination of N-AC in drug and urine samples.

English

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  • 发布日期:  2014-04-20
  • 收稿日期:  2013-11-17
  • 网络出版日期:  2013-12-27
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