Citation:
Khalil Faghihi, Hassan Moghanian. SYNTHESIS AND CHARACTERIZATION OF OPTICALLY ACTIVE POLY(AMIDE-IMIDE)S CONTAINING PHOTOSENSITIVE CHALCONE UNITS IN THE MAIN CHAIN[J]. Chinese Journal of Polymer Science,
2010, 28(5): 695-704.
doi:
10.1007/s10118-010-9119-5
SYNTHESIS AND CHARACTERIZATION OF OPTICALLY ACTIVE POLY(AMIDE-IMIDE)S CONTAINING PHOTOSENSITIVE CHALCONE UNITS IN THE MAIN CHAIN
摘要:
A series of new optically active poly(amide-imide)s were synthesized by direct polycondensation reaction of 4,4'-diaminochalcone with several N-trimellitylimido-L-amino acids using a tosyl chloride (TsCl), pyridine (Py) and dimethylformamide (DMF) system as condensing agent. The resulting thermally stable poly(amide-imide)s were obtained in good to high yields and inherent viscosities ranging between 0.35 dL/g and 0.58 dL/g and were characterized with FTIR, 1H-NMR, CHN, Ultraviolet, TGA and DTG techniques.
English
SYNTHESIS AND CHARACTERIZATION OF OPTICALLY ACTIVE POLY(AMIDE-IMIDE)S CONTAINING PHOTOSENSITIVE CHALCONE UNITS IN THE MAIN CHAIN
Abstract:
A series of new optically active poly(amide-imide)s were synthesized by direct polycondensation reaction of 4,4'-diaminochalcone with several N-trimellitylimido-L-amino acids using a tosyl chloride (TsCl), pyridine (Py) and dimethylformamide (DMF) system as condensing agent. The resulting thermally stable poly(amide-imide)s were obtained in good to high yields and inherent viscosities ranging between 0.35 dL/g and 0.58 dL/g and were characterized with FTIR, 1H-NMR, CHN, Ultraviolet, TGA and DTG techniques.
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