引用本文:
成康民, 沈玉梅, 王谋华, 冯翠兰. β-榄香烯氨基酸衍生物的合成[J]. 应用化学,
2008, 25(5): 560-563.
Citation: CHENG Kang-Min, SHEN Yu-Mei, WANG Mou-Hua, FENG Cui-Lan. Synthesis of β-Elemene Amino Acid Derivatives[J]. Chinese Journal of Applied Chemistry, 2008, 25(5): 560-563.
Citation: CHENG Kang-Min, SHEN Yu-Mei, WANG Mou-Hua, FENG Cui-Lan. Synthesis of β-Elemene Amino Acid Derivatives[J]. Chinese Journal of Applied Chemistry, 2008, 25(5): 560-563.
β-榄香烯氨基酸衍生物的合成
English
Synthesis of β-Elemene Amino Acid Derivatives
Abstract:
A series of β-elemene monosubstituted amino acid derivatives were synthesized from the reaction of β-elemene with each of seven different amino acids under basic condition at 66℃,and their structures were characterized by IR,1H NMR,and HRMS.Sodium hypochloride added in this step should be 2 equivalent of the reacted β-elemene.The β-elemene monosubstituted amino acid derivatives were prepared from the unprotected amino acids with ethanol and water as solvent (V(EtOH):V(H2O)=4:1).The effects of temperature on reaction yield showed that more byproducts would appear at higher temperatures and the reaction would run much slower at low temperatures.
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Key words:
- β-elemene
- / derivatives
- / amino acid
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