引用本文:
周立群, 杨念华, 周丽荣, 孙聚堂. 纳米氧化镍的固相合成[J]. 应用化学,
2006, 23(6): 682-684.
Citation: ZHOU Li-Qun, YANG Nian-Hua, ZHOU Li-Rong, SUN Ju-Tang. Preparation and Formation Mechanism of NiO Nanoparticles by Solid State Reaction[J]. Chinese Journal of Applied Chemistry, 2006, 23(6): 682-684.

Citation: ZHOU Li-Qun, YANG Nian-Hua, ZHOU Li-Rong, SUN Ju-Tang. Preparation and Formation Mechanism of NiO Nanoparticles by Solid State Reaction[J]. Chinese Journal of Applied Chemistry, 2006, 23(6): 682-684.

纳米氧化镍的固相合成
English
Preparation and Formation Mechanism of NiO Nanoparticles by Solid State Reaction
Abstract:
NiO nanoparticles were successfully prepared by solid state thermal decomposition of NiCO3 (10 nm) precursor,which was synthesized by solid state reaction at room temperature.The crystal structure,particle-size and properties of the nanoparticles were characterized by means of XRD,TEM TG-DTA and BET.The results show that the NiO had an average particle size of 5.8 nm and highest BET specific surface area of 116.6 m2/g after annealling the precursor at 300℃ for 2 h.The formation mechanism of the nanoparticles were also discussed.
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Key words:
- NiO
- / nanoparticle
- / solid state reaction
- / synthesis mechanism
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